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ChemicalBook >> CAS DataBase List >>tert-butyl 2-bromo-6,7-dihydrothiazolo[5,4-c]pyridine-5(4H)-carboxylate

tert-butyl 2-bromo-6,7-dihydrothiazolo[5,4-c]pyridine-5(4H)-carboxylate

CAS No.
365996-06-1
Chemical Name:
tert-butyl 2-bromo-6,7-dihydrothiazolo[5,4-c]pyridine-5(4H)-carboxylate
Synonyms
tert-butyl 2-broMo-6;5-Boc-2-bromo-6,7-dihydro-4H-thiazolo[5,4-c]pyridine;tert-Butyl 2-bromo-6,7-dihydrothiazolo[5,4-c]pyridine-5(4H);tert-butyl 2-bromo-6,7-dihydro-4H-thiazolo[5,4-c]pyridine-5-...;tert-Butyl 2-bromo-6,7-dihydrothiazolo[5,4-c]pyridin-5(4H)-carboxylate;2-Bromo-4,5,6,7-tetrahydro[1,3]thiazolo[5,4-c]pyridine, N-BOC protected;tert-butyl 2-broMo-6,7-dihydro-4H-thiazolo[5,4-c]pyridine-5-carboxylate;tert-butyl 2-bromo-6,7-dihydrothiazolo[5,4-c]pyridine-5(4H)-carboxylate;tert-butyl 2-broMo-4H,5H,6H,7H-[1,3]thiazolo[5,4- c]pyridine-5-carboxylate;tert-butyl 2-bromo-6,7-dihydro-4H-[1,3]thiazolo[5,4-c]pyridine-5-carboxylate
CBNumber:
CB01856206
Molecular Formula:
C11H15BrN2O2S
Molecular Weight:
319.22
MDL Number:
MFCD09951958
MOL File:
365996-06-1.mol
MSDS File:
SDS
Last updated:2026-05-27 17:24:51
Product description Number Pack Size Price
2-Bromo-5-(tert-butoxycarbonyl)-4,5,6,7-tetrahydrothiazolo[5,4-c]pyridine 415985 100mg $326
2-Bromo-5-(tert-butoxycarbonyl)-4,5,6,7-tetrahydrothiazolo[5,4-c]pyridine 415985 250mg $482
5-BOC-2-BROMO-6,7-DIHYDRO-4H-THIAZOLO-[5,4,C]PYRIDINE 95% AB1021 0.25G $20
5-BOC-2-BROMO-6,7-DIHYDRO-4H-THIAZOLO-[5,4,C]PYRIDINE 95% AB1021 1G $27
5-BOC-2-BROMO-6,7-DIHYDRO-4H-THIAZOLO-[5,4,C]PYRIDINE 95% AB1021 5G $79
More product size

tert-butyl 2-bromo-6,7-dihydrothiazolo[5,4-c]pyridine-5(4H)-carboxylate Properties

Melting point 42-44 °C(Solv: ethyl ether (60-29-7))
Boiling point 390.9±42.0 °C(Predicted)
Density 1.495±0.06 g/cm3(Predicted)
storage temp. under inert gas (nitrogen or Argon) at 2-8°C
pka 1.23±0.20(Predicted)
Appearance White to off-white Solid
InChI InChI=1S/C11H15BrN2O2S/c1-11(2,3)16-10(15)14-5-4-7-8(6-14)17-9(12)13-7/h4-6H2,1-3H3
InChIKey RXXKNZKFRAFFOH-UHFFFAOYSA-N
SMILES C1N(C(OC(C)(C)C)=O)CCC2N=C(Br)SC1=2

SAFETY

Risk and Safety Statements

Symbol(GHS)  Exclamation Mark (GHS07)
GHS07
Signal word  Warning
Hazard statements  H315-H319-H335
Precautionary statements  P261-P305+P351+P338
Hazard Codes  T
Risk Statements  25
Safety Statements  45
RIDADR  UN2811
HS Code  2934100090

tert-butyl 2-bromo-6,7-dihydrothiazolo[5,4-c]pyridine-5(4H)-carboxylate price More Price(65)

Manufacturer Product number Product description CAS number Packaging Price Updated Buy
Usbiological 415985 2-Bromo-5-(tert-butoxycarbonyl)-4,5,6,7-tetrahydrothiazolo[5,4-c]pyridine 365996-06-1 100mg $326 2026-06-03 Buy
Usbiological 415985 2-Bromo-5-(tert-butoxycarbonyl)-4,5,6,7-tetrahydrothiazolo[5,4-c]pyridine 365996-06-1 250mg $482 2026-06-03 Buy
AstaTech AB1021 5-BOC-2-BROMO-6,7-DIHYDRO-4H-THIAZOLO-[5,4,C]PYRIDINE 95% 365996-06-1 0.25G $20 2026-04-30 Buy
AstaTech AB1021 5-BOC-2-BROMO-6,7-DIHYDRO-4H-THIAZOLO-[5,4,C]PYRIDINE 95% 365996-06-1 1G $27 2026-04-30 Buy
AstaTech AB1021 5-BOC-2-BROMO-6,7-DIHYDRO-4H-THIAZOLO-[5,4,C]PYRIDINE 95% 365996-06-1 5G $79 2026-04-30 Buy
Product number Packaging Price Buy
415985 100mg $326 Buy
415985 250mg $482 Buy
AB1021 0.25G $20 Buy
AB1021 1G $27 Buy
AB1021 5G $79 Buy

tert-butyl 2-bromo-6,7-dihydrothiazolo[5,4-c]pyridine-5(4H)-carboxylate Chemical Properties,Uses,Production

Uses

2-Bromo-5-(tert-butoxycarbonyl)-4,5,6,7-tetrahydrothiazolo[5,4-c]pyridine is a reagent used for the synthesis of tetrahydrothiazolopyridines, which are potent antagonists for the smoothened (smo) receptor.

Uses

2-Bromo-5-(tert-butoxycarbonyl)-4,5,6,7-tetrahydrothiazolo[5,4-c]pyridine is a reagent used for the synthesis of tetrahydrothiazolopyridines, which are potent antagonists for the smoothened (smo) receptor.

Synthesis

TERT-BUTYL 2-AMINO-6,7-DIHYDROTHIAZOLO[5,4-C]PYRIDINE-5(4H)-CARBOXYLATE

365996-05-0

tert-butyl 2-bromo-6,7-dihydrothiazolo[5,4-c]pyridine-5(4H)-carboxylate

365996-06-1

Method G - Step e: Synthesis of tert-butyl 2-bromo-6,7-dihydrothiazolo[5,4-c]pyridine-5(4H)-carboxylate [0134] To a 100 mL DMF solution containing isoamyl nitrite (8.8 mL, 62.8 mmol) and copper(II) bromide (10.7 g, 48 mmol) was added tert-butyl 2-amino-6,7-dihydrothiazolo[5,4-c]pyridine-5(4H)-carboxylate (10 g, 39.2 mmol) at 0°C. The reaction was carried out at 40°C and the reaction mixture was purified. The reaction mixture was stirred at 40°C for 30 min and then concentrated by evaporation. The concentrate was dissolved in 50 mL of water and extracted with dichloromethane (100 mL × 2). The organic phases were combined, washed with brine (30 mL × 2), and dried over anhydrous sodium sulfate. Purification by silica gel column chromatography (eluent: dichloromethane) afforded the target product tert-butyl 2-bromo-6,7-dihydrothiazolo[5,4-c]pyridine-5(4H)-carboxylate (5.3 g, 42.4%) as a yellow solid.

References

[1] Heterocycles, 2004, vol. 63, # 7, p. 1555 - 1561
[2] Patent: WO2014/113191, 2014, A1. Location in patent: Paragraph 0133; 0134
[3] Patent: US2013/144061, 2013, A1. Location in patent: Paragraph 0244; 0245; 0246; 0247
[4] Journal of Medicinal Chemistry, 2014, vol. 57, # 9, p. 3687 - 3706
[5] Patent: WO2018/13774, 2018, A1. Location in patent: Page/Page column 309

540-80-7
365996-05-0
365996-06-1
Synthesis of tert-butyl 2-bromo-6,7-dihydrothiazolo[5,4-c]pyridine-5(4H)-carboxylate from tert-Butyl nitrite and TERT-BUTYL 2-AMINO-6,7-DIHYDROTHIAZOLO[5,4-C]PYRIDINE-5(4H)-CARBOXYLATE
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View Lastest Price from tert-butyl 2-bromo-6,7-dihydrothiazolo[5,4-c]pyridine-5(4H)-carboxylate manufacturers

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tert-butyl 2-bromo-6,7-dihydrothiazolo[5,4-c]pyridine-5(4H)-carboxylate pictures 2020-01-08 tert-butyl 2-bromo-6,7-dihydrothiazolo[5,4-c]pyridine-5(4H)-carboxylate
365996-06-1
 $5.50 1KG 98%-99% 1kg-100kg Career Henan Chemical Co

tert-butyl 2-bromo-6,7-dihydrothiazolo[5,4-c]pyridine-5(4H)-carboxylate Spectrum

365996-06-1(tert-butyl 2-bromo-6,7-dihydrothiazolo[5,4-c]pyridine-5(4H)-carboxylate)Related Search:

tert-butyl 2-bromo-6,7-dihydrothiazolo[5,4-c]pyridine-5(4H)-carboxylate tert-butyl 2-bromo-6,7-dihydro[1,3]thiazolo[5,4-c]pyridine-5(4H)-carboxylate tert-butyl 2-broMo-6 2-BroMo-6,7-dihydro-4H-thiazolo[5,4-c]pyridine-5-carboxylicacidtert-butylester 2-Bromo-4,5,6,7-tetrahydro[1,3]thiazolo[5,4-c]pyridine, N-BOC protected Thiazolo[5,4-c]pyridine-5(4H)-carboxylic acid, 2-broMo-6,7-dihydro-, 1,1-diMethylethyl ester tert-butyl 2-broMo-4H,5H,6H,7H-[1,3]thiazolo[5,4- c]pyridine-5-carboxylate 5-Boc-2-bromo-6,7-dihydro-4H-thiazolo[5,4-c]pyridine tert-butyl 2-broMo-6,7-dihydro-4H-thiazolo[5,4-c]pyridine-5-carboxylate tert-butyl 2-bromo-6,7-dihydro-4H-[1,3]thiazolo[5,4-c]pyridine-5-carboxylate tert-Butyl 2-bromo-6,7-dihydrothiazolo[5,4-c]pyridine-5(4H) tert-butyl 2-bromo-6,7-dihydro-4H-thiazolo[5,4-c]pyridine-5-... 1,1-Dimethylethyl 2-bromo-6,7-dihydrothiazolo[5,4-c]pyridine-5(4H)-carboxylate tert-Butyl 2-bromo-6,7-dihydrothiazolo[5,4-c]pyridin-5(4H)-carboxylate 365996-06-1 CHIRAL CHEMICALS Heterocycle-Pyridine series
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