2,4-DICHLOROPHENETHYL ALCOHOL
- CAS No.
- 81156-68-5
- Chemical Name:
- 2,4-DICHLOROPHENETHYL ALCOHOL
- Synonyms
- 2-(2,4-dichlorophenyl)ethan-1-ol;2,4-Dichlorobenzeneethanol;2-(2,4-DICHLOROPHENYL)ETHANOL;2,4-DICHLOROPHENETHYL ALCOHOL;Benzeneethanol, 2,4-dichloro-;2-(2,4-Dichlorophenyl)ethanol>2,4-Dichlorophenethyl alcohol,98%;2,4-Dichlorophenethyl alcohol 97%;2,4-Dichlorophenethyl alcohol, 98% 5GR
- CBNumber:
- CB2419798
- Molecular Formula:
- C8H8Cl2O
- Molecular Weight:
- 191.05
- MDL Number:
- MFCD00192010
- MOL File:
- 81156-68-5.mol
- MSDS File:
- SDS
| Product description | Number | Pack Size | Price |
| 2,4-Dichlorophenethyl alcohol 97% | 394556 | 1g | $32.9 |
| 2,4-Dichlorophenethyl alcohol 97% | 394556 | 5g | $66 |
| 2-(2,4-Dichlorophenyl)ethanol >97.0%(GC) | D2921 | 5g | $39 |
| 2-(2,4-Dichlorophenyl)ethanol | FD64476 | 10g | $150 |
| 2-(2,4-Dichlorophenyl)ethanol | FD64476 | 25g | $181.5 |
| More product size | |||
| Boiling point | 119 °C/0.8 mmHg (lit.) |
|---|---|
| Density | 1.321 g/mL at 25 °C (lit.) |
| refractive index |
n |
| Flash point | >230 °F |
| storage temp. | Sealed in dry,Room Temperature |
| form | Liquid |
| pka | 14.57±0.10(Predicted) |
| Specific Gravity | 1.321 |
| color | Clear colorless |
| InChI | 1S/C8H8Cl2O/c9-7-2-1-6(3-4-11)8(10)5-7/h1-2,5,11H,3-4H2 |
| InChIKey | JIJGKPVJAALUQQ-UHFFFAOYSA-N |
| SMILES | OCCc1ccc(Cl)cc1Cl |
| CAS DataBase Reference | 81156-68-5 |
| UNSPSC Code | 12352100 |
SAFETY
Risk and Safety Statements
| Symbol(GHS) |  GHS07 |
|||||||||
|---|---|---|---|---|---|---|---|---|---|---|
| Signal word | Warning | |||||||||
| Hazard statements | H315-H319-H335 | |||||||||
| Precautionary statements | P261-P305+P351+P338 | |||||||||
| PPE | Eyeshields, Gloves | |||||||||
| Safety Statements | 24/25 | |||||||||
| WGK Germany | 3 | |||||||||
| HS Code | 29062990 | |||||||||
| Storage Class | 10 - Combustible liquids | |||||||||
| NFPA 704 |
|
2,4-DICHLOROPHENETHYL ALCOHOL price More Price(56)
| Manufacturer | Product number | Product description | CAS number | Packaging | Price | Updated | Buy |
|---|---|---|---|---|---|---|---|
| Sigma-Aldrich | 394556 | 2,4-Dichlorophenethyl alcohol 97% | 81156-68-5 | 1g | $32.9 | 2023-01-07 | Buy |
| Sigma-Aldrich | 394556 | 2,4-Dichlorophenethyl alcohol 97% | 81156-68-5 | 5g | $66 | 2023-01-07 | Buy |
| TCI Chemical | D2921 | 2-(2,4-Dichlorophenyl)ethanol >97.0%(GC) | 81156-68-5 | 5g | $39 | 2026-04-30 | Buy |
| Biosynth | FD64476 | 2-(2,4-Dichlorophenyl)ethanol | 81156-68-5 | 10g | $150 | 2026-06-04 | Buy |
| Biosynth | FD64476 | 2-(2,4-Dichlorophenyl)ethanol | 81156-68-5 | 25g | $181.5 | 2026-06-04 | Buy |
2,4-DICHLOROPHENETHYL ALCOHOL Chemical Properties,Uses,Production
Chemical Properties
clear colorless liquid
Uses
2,4-Dichlorophenethyl alcohol is a phenethyl alcohol derivative. Its selective electrocatalytic dehalogenation over Pd-loaded felt cathode has been investigated.
General Description
2,4-Dichlorophenethyl alcohol is a phenethyl alcohol derivative. Its selective electrocatalytic dehalogenation over Pd-loaded felt cathode has been investigated.
Synthesis
50-00-0
94-99-5
81156-68-5
The general procedure for the synthesis of 2,4-dichlorophenethyl alcohol from formaldehyde and 2,4-dichlorobenzyl chloride is as follows: a two-necked Schlenk flask equipped with a magnetic stirring bar and a septum is heated under high vacuum with a hot air gun (ca. 400 °C) for 10 minutes. After cooling to room temperature, the flask was rinsed three times with argon. Zinc powder (654 mg, 2.0 equiv, 10.0 mmol) and THF (20 mL) were added sequentially. 1,2-Dibromoethane (5 mol%) was added and the reaction mixture was heated to boiling. After cooling to room temperature, chlorotrimethylsilane (1 mol%) was added and the mixture was again heated to boiling. After cooling to room temperature again, a solution of 2,4-dichlorobenzyl chloride (633 mg, 5.0 mmol, 1 eq.) in THF (10 mL) was added and the reaction mixture was heated at 70 °C for 2 hours and then cooled to room temperature. Paraformaldehyde (450 mg, 3.0 eq., 15.0 mmol) was slowly added at room temperature and the flask was heated again at 70 °C for 6 hours. After completion of the reaction, the solution was cooled to room temperature and saturated NH4Cl solution was added. The organic and aqueous phases were separated and the aqueous phase was extracted with ethyl acetate (100 mL). The organic layers were combined and washed sequentially with water (20 mL) and brine (10 mL), then dried with Na2SO4. The solvent was evaporated under reduced pressure and the residue was purified by silica gel column chromatography using cyclohexane or cyclohexane/ethyl acetate as eluent to afford 2,4-dichlorobenzeneethanol (510 mg, 83% yield) as a colorless liquid.
References
[1] Synthetic Communications, 2017, vol. 47, # 10, p. 968 - 974
2,4-DICHLOROPHENETHYL ALCOHOL Preparation Products And Raw materials
Raw materials
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Preparation Products
| Supplier | Tel | Country | ProdList | Advantage | |
|---|---|---|---|---|---|
| Alchem Pharmtech,Inc. | 8485655694 | sales@alchempharmtech.com | United States | 63687 | 58 |
| CONIER CHEM AND PHARMA LIMITED | +8618523575427 | sales@conier.com | China | 49979 | 58 |
| career henan chemical co | +86-0371-86658258 +8613203830695 | factory@coreychem.com | China | 29792 | 58 |
| Fuxin Pharmaceutical | +86-021-021-50872116 +8613122107989 | contact@fuxinpharm.com | China | 10000 | 58 |
| Guangzhou Yuheng Pharmaceutical Technology Co., Ltd | +8613580539051 | joe@yuhengpharm.com | CHINA | 21142 | 58 |
| Win-Win chemical CO., Limited | +86-0086-577-64498589 +86-15355981851 | sales@win-winchemical.com | China | 14304 | 58 |
| Shanxi Xuanran Import and Export Trade Co., Ltd. | +8617735180244 | mike_yan@xuanranglobal.com | CHINA | 4017 | 58 |
| Dayang Chem (Hangzhou) Co.,Ltd. | +86-0571-88938639 +8617705817739 | info@dycnchem.com | China | 52704 | 58 |
| CD Chemical Group Limited | +8615986615575 | info@codchem.com | China | 17259 | 58 |
| Changzhou Fullone Chemical Co., Ltd. | +86-13328197671 +86-13861172460 | sales@borenchem.cn | China | 1055 | 58 |
View Lastest Price from 2,4-DICHLOROPHENETHYL ALCOHOL manufacturers
| Image | Update time | Product | Price | Min. Order | Purity | Supply Ability | Manufacturer | |
|---|---|---|---|---|---|---|---|---|
 |
2019-12-25 | 2,4-DICHLOROPHENETHYL ALCOHOL
81156-68-5
|
$1.00 | 1KG | 99% | 200kg | Career Henan Chemical Co |
-
- 2,4-DICHLOROPHENETHYL ALCOHOL
81156-68-5
- $1.00
- 99%
- Career Henan Chemical Co
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