1,10-Dibromodecane
- CAS No.
- 4101-68-2
- Chemical Name:
- 1,10-Dibromodecane
- Synonyms
- DECAMETHYLENE DIBROMIDE;,w-Dibromodecane;Dibromodecane,95%;1,10-DIBROMODECANE;1,10-dibromo-decan;TIMTEC-BB SBB008900;Decene, 1,10-dibromo;DECAMETHYLENE BROMIDE;Decane, 1,10-dibromo-;1,10-DECANE DIBROMIDE
- CBNumber:
- CB3322169
- Molecular Formula:
- C10H20Br2
- Molecular Weight:
- 300.07
- MDL Number:
- MFCD00000222
- MOL File:
- 4101-68-2.mol
- MSDS File:
- SDS
| Product description | Number | Pack Size | Price |
| 1,10-Dibromodecane 97% | D39800 | 100g | $132 |
| 1,10-Dibromodecane >95.0%(GC) | D0179 | 25g | $27 |
| 1,10-Dibromodecane >95.0%(GC) | D0179 | 100g | $94 |
| 1,10-Dibromodecane 97% | J99517 | 5g | $13 |
| 1,10-Dibromodecane 97% | J99517 | 25g | $23 |
| More product size | |||
| Melting point | 25-27 °C (lit.) |
|---|---|
| Boiling point | 160 °C/15 mmHg (lit.) |
| Density | 1.335 g/mL at 25 °C (lit.) |
| refractive index |
n |
| Flash point | 26°C |
| storage temp. | Sealed in dry,Room Temperature |
| form | Crystalline Low Melting Solid |
| Specific Gravity | 1.335 |
| color | Beige to brown |
| Water Solubility | insoluble |
| BRN | 506156 |
| Dielectric constant | 6.5599999999999996 |
| InChI | 1S/C10H20Br2/c11-9-7-5-3-1-2-4-6-8-10-12/h1-10H2 |
| InChIKey | GTQHJCOHNAFHRE-UHFFFAOYSA-N |
| SMILES | BrCCCCCCCCCCBr |
| CAS DataBase Reference | 4101-68-2(CAS DataBase Reference) |
| NIST Chemistry Reference | Decane, 1,10-dibromo-(4101-68-2) |
| EPA Substance Registry System | Decane, 1,10-dibromo- (4101-68-2) |
| UNSPSC Code | 12352100 |
| NACRES | NA.22 |
SAFETY
Risk and Safety Statements
| Symbol(GHS) |  GHS07 |
|||||||||
|---|---|---|---|---|---|---|---|---|---|---|
| Signal word | Warning | |||||||||
| Hazard statements | H302-H315-H319-H335 | |||||||||
| Precautionary statements | P261-P305+P351+P338 | |||||||||
| PPE | Eyeshields, Gloves, type N95 (US) | |||||||||
| Hazard Codes | C,Xi | |||||||||
| Risk Statements | 20/21/22-36/37/38 | |||||||||
| Safety Statements | 22-24/25-36-26 | |||||||||
| WGK Germany | 3 | |||||||||
| TSCA | TSCA listed | |||||||||
| HS Code | 29049090 | |||||||||
| Storage Class | 11 - Combustible Solids | |||||||||
| REACH Registrations | Active | |||||||||
| NFPA 704 |
|
1,10-Dibromodecane price More Price(47)
| Manufacturer | Product number | Product description | CAS number | Packaging | Price | Updated | Buy |
|---|---|---|---|---|---|---|---|
| Sigma-Aldrich | D39800 | 1,10-Dibromodecane 97% | 4101-68-2 | 100g | $132 | 2026-04-30 | Buy |
| TCI Chemical | D0179 | 1,10-Dibromodecane >95.0%(GC) | 4101-68-2 | 25g | $27 | 2026-04-30 | Buy |
| TCI Chemical | D0179 | 1,10-Dibromodecane >95.0%(GC) | 4101-68-2 | 100g | $94 | 2026-04-30 | Buy |
| AK Scientific | J99517 | 1,10-Dibromodecane 97% | 4101-68-2 | 5g | $13 | 2026-06-04 | Buy |
| AK Scientific | J99517 | 1,10-Dibromodecane 97% | 4101-68-2 | 25g | $23 | 2026-06-04 | Buy |
1,10-Dibromodecane Chemical Properties,Uses,Production
Chemical Properties
beige to brown crystalline low melting mass
Uses
1,10-Dibromodecane is used as an alkylating agent and as synthetic organic intermediate.
Synthesis
112-47-0
4101-68-2
The general procedure for the synthesis of 1,10-dibromodecane from 1,10-decanediol is as follows: 1,10-decanediol (1 eq.), 48% aqueous hydrobromic acid (ca. 3 eq./hydroxyl), and octane (ca. 7:1 volume-to-weight ratio to the diol) were added to a single-necked, round-bottomed flask and assembled with a fractionating column/Dean-Stark trap. The reaction mixture was placed in a heated oil bath (145-150°C) with rapid magnetic stirring. The aqueous (lower) layer at the initial boiling point (89-92°C) was condensed and gently separated, and subsequently collected at about half the theoretical volume of water; at this point the temperature of the azeotrope (still at head temperature) began to rise. The condenser was set to full reflux for a few hours, then turned back on and the aqueous-phase material continued to be collected for 1 hour (top temperature 96-100°C). The final volume of the aqueous phase distillate reaches 90-100% of the theoretical value (up to 24% hydrobromic acid in the high boiling distillate). When the octane phase (which is light tan in color) contains dibromides and brominated streptanols (e.g., 6 band 6c), it is washed with cold 85% v/v sulfuric acid (10 mL first, then 5 mL) to remove all color and brominated streptanols. For all three dibromides (3b, 4b, 6b), the neutralized octane solution was passed through a Vigreux column under reduced pressure to remove the solvent, and the residue (which was confirmed to be essentially pure by 1H NMR) was purified by Kugelrohr distillation. Trace amounts of 4-methyltetrahydropyran were detected prior to distillation of 4b.
References
[1] Tetrahedron Letters, 2015, vol. 56, # 4, p. 630 - 632
[2] Green Chemistry, 2014, vol. 16, # 2, p. 836 - 843
[3] Journal of Organic Chemistry, 2015, vol. 80, # 11, p. 5386 - 5394
[4] Journal of the American Chemical Society, 1936, vol. 58, p. 488
[5] Journal of the Chemical Society, 1958, p. 2068
1,10-Dibromodecane Preparation Products And Raw materials
Raw materials
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Preparation Products
1of2
| Supplier | Tel | Country | ProdList | Advantage | |
|---|---|---|---|---|---|
| Yancheng Longshen Chemical Co.,Ltd. | +86-18352073383 +86-18352073383 | sales@longshenchem.com | China | 100 | 55 |
| Hebei Yanxi Chemical Co., Ltd. | +8618531123677 | faithe@yan-xi.com | China | 5853 | 58 |
| Hebei Chuanghai Biotechnology Co,.LTD | +86-86-13131129325 +8613131129325 | sales1@chuanghaibio.com | China | 5228 | 58 |
| Hebei Chuanghai Biotechnology Co., Ltd | +8615531151365 | mina@chuanghaibio.com | China | 18126 | 58 |
| Firsky International Trade (Wuhan) Co., Ltd | +8615387054039 | admin@firsky-cn.com | China | 427 | 58 |
| Henan Fengda Chemical Co., Ltd | +86-371-86557731 +86-13613820652 | info@fdachem.com | China | 20122 | 58 |
| Shanghai Daken Advanced Materials Co.,Ltd | +86-2158073036 | info@dakenam.com | China | 13901 | 58 |
| Henan Tianfu Chemical Co.,Ltd. | +86-0371-55170693 +86-19937530512 | info@tianfuchem.com | China | 21587 | 55 |
| Xiamen AmoyChem Co., Ltd | +86-86-5926051114 +8615060885618 | sales@amoychem.com | China | 6366 | 58 |
| Alchem Pharmtech,Inc. | 8485655694 | sales@alchempharmtech.com | United States | 63687 | 58 |
View Lastest Price from 1,10-Dibromodecane manufacturers
| Image | Update time | Product | Price | Min. Order | Purity | Supply Ability | Manufacturer | |
|---|---|---|---|---|---|---|---|---|
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2026-06-06 | 1,10-Dibromodecane
4101-68-2
|
1KG | ≥98.5% | 20 Tons/Month | Yancheng Longshen Chemical Co.,Ltd. | ||
 |
2026-05-28 | 1,10-dibromodecane
4101-68-2
|
$1.00 | 1KG | 99.% | 50 ton | Hebei Chuanghai Biotechnology Co,.LTD | |
 |
2025-09-25 | 1,10-Dibromodecane
4101-68-2
|
$1.00-100.00 | 1KG | 99% | Henan Fengda Chemical Co., Ltd |
-
- 1,10-Dibromodecane
4101-68-2
- $0.00
- ≥98.5%
- Yancheng Longshen Chemical Co.,Ltd.
-
- 1,10-dibromodecane
4101-68-2
- $1.00
- 99.%
- Hebei Chuanghai Biotechnology Co,.LTD
-
- 1,10-Dibromodecane
4101-68-2
- $1.00-100.00
- 99%
- Henan Fengda Chemical Co., Ltd
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