6-bromo-7-methylquinoline
- CAS No.
- 122759-89-1
- Chemical Name:
- 6-bromo-7-methylquinoline
- Synonyms
- 6-bromo-7-methylquinoline;Quinoline, 6-bromo-7-methyl-
- CBNumber:
- CB82537630
- Molecular Formula:
- C10H8BrN
- Molecular Weight:
- 222.08
- MDL Number:
- MFCD18260428
- MOL File:
- 122759-89-1.mol
- MSDS File:
- SDS
| Product description | Number | Pack Size | Price |
| 6-Bromo-7-methylquinoline >97% | OR43652 | 1g | $30 |
| 6-Bromo-7-methylquinoline >97% | OR43652 | 5g | $135 |
| 6-Bromo-7-methylquinoline >97% | OR43652 | 25g | $615 |
| 6-Bromo-7-methylquinoline 97% | AS110086 | 1g | $61 |
| 6-Bromo-7-methylquinoline 97% | AS110086 | 5g | $162 |
SAFETY
Risk and Safety Statements
| Symbol(GHS) |    GHS05,GHS07,GHS08 |
|---|---|
| Signal word | Danger |
| Hazard statements | H302-H315-H317-H318-H334-H335 |
| Precautionary statements | P280-P301+P312-P261 |
| HS Code | 2933499090 |
6-bromo-7-methylquinoline price More Price(44)
| Manufacturer | Product number | Product description | CAS number | Packaging | Price | Updated | Buy |
|---|---|---|---|---|---|---|---|
| Apolloscientific | OR43652 | 6-Bromo-7-methylquinoline >97% | 122759-89-1 | 1g | $30 | 2026-06-04 | Buy |
| Apolloscientific | OR43652 | 6-Bromo-7-methylquinoline >97% | 122759-89-1 | 5g | $135 | 2026-06-04 | Buy |
| Apolloscientific | OR43652 | 6-Bromo-7-methylquinoline >97% | 122759-89-1 | 25g | $615 | 2026-06-04 | Buy |
| Activate Scientific | AS110086 | 6-Bromo-7-methylquinoline 97% | 122759-89-1 | 1g | $61 | 2026-06-04 | Buy |
| Activate Scientific | AS110086 | 6-Bromo-7-methylquinoline 97% | 122759-89-1 | 5g | $162 | 2026-06-04 | Buy |
6-bromo-7-methylquinoline Chemical Properties,Uses,Production
Chemical Properties
Yellow solid
Synthesis
6933-10-4
56-81-5
122759-89-1
General procedure for the synthesis of 6-bromo-7-methylquinoline from 4-bromo-3-methylaniline and glycerol: [0304] A mixture of 4-bromo-3-methylaniline (20 g, 107.5 mmol), ferric sulfate (6.6 g, 43.4 mmol), glycerol (40.8 g, 440 mmol) and nitrobenzene (8.12 g, 66 mmol) was mixed with concentrated sulfuric acid (23 ml) and slowly heated. After the initial vigorous reaction subsided, the reaction mixture was refluxed for 3 h. The excess nitrobenzene was subsequently removed by evaporation. The pH was adjusted to 7-8 by adding saturated aqueous sodium bicarbonate solution to the reaction mixture and then filtered. The filtrate was extracted with dichloromethane and the organic layers were combined and dried over anhydrous sodium sulfate. The dried organic phase was filtered and concentrated in vacuum and the resulting solid was purified by fast column chromatography. The purified yellow solid was further washed with petroleum ether to afford 7.5 g of 6-bromo-7-methylquinoline in 31% yield. The structure of the product was confirmed by 1H NMR (CDCl3): δ 2.60 (s, 3H), 7.36 (m, 1H), 7.96 (s, 1H), 8.04 (m, 2H), 8.89 (m, 1H).
References
[1] Patent: WO2008/51808, 2008, A2. Location in patent: Page/Page column 79-80
6-bromo-7-methylquinoline Preparation Products And Raw materials
Raw materials
1of2
Preparation Products
6-bromo-7-methylquinoline Suppliers
| Supplier | Tel | Country | ProdList | Advantage | |
|---|---|---|---|---|---|
| Dayang Chem (Hangzhou) Co.,Ltd. | +86-0571-88938639 +8617705817739 | info@dycnchem.com | China | 52704 | 58 |
| CR Corporation Limited | +8613062833949 | fred.wen@crcorporation.cn | China | 8645 | 58 |
| GIHI CHEMICALS CO.,LIMITED | +86-571-86217390; +8618058761490 | info@gihichemicals.com | China | 49962 | 58 |
| Aladdin Scientific | tp@aladdinsci.com | United States | 57505 | 58 | |
| Amadis Chemical Company Limited | 571-89925085 | sales@amadischem.com | China | 131956 | 58 |
| Henan Rane Chemical Co., Ltd. | +8618738066252 | info@ranechem.com | China | 3000 | 58 |
| Adamas Reagent, Ltd. | 400-6009262 15618770481 | yhx@titansci.com | China | 14100 | 59 |
| Shandong Xiya Chemical Co., Ltd | 13355009207 13355009207 | 3007715519@qq.com | China | 18728 | 57 |
| Shanghai Sunway Pharmaceutical Technology Co., Ltd | 13761987713 | hxzheng@sunwaypharm.cn | China | 8666 | 57 |
| Chengdu Forest Science and Technology Development Co., Ltd. | 18030648795 18030648795 | sales@cdforestchem.com | China | 1996 | 58 |
