1-Boc-3-piperidone
- CAS No.
- 98977-36-7
- Chemical Name:
- 1-Boc-3-piperidone
- Synonyms
- TERT-BUTYL 3-OXOPIPERIDINE-1-CARBOXYLATE;N-Boc-3-piperidone;N-BOC-3-PIPERIDINONE;3-OXO-PIPERIDINE-1-CARBOXYLIC ACID TERT-BUTYL ESTER;1-BOC-piperidone;1-BOC-3-PIPERIDINONE;1-(TERT-BUTOXYCARBONYL)-3-PIPERIDONE;1-Boc-3-Pipe;3-Oxopiperidine;BOC-3-PIPERIDONE
- CBNumber:
- CB8428473
- Molecular Formula:
- C10H17NO3
- Molecular Weight:
- 199.25
- MDL Number:
- MFCD01631193
- MOL File:
- 98977-36-7.mol
- MSDS File:
- SDS
- TDS File:
- TDS
| Product description | Number | Pack Size | Price |
| 1-Boc-3-piperidone 97% | 650811 | 25g | $80.7 |
| 1-Boc-3-piperidone 97% | 650811 | 5g | $30 |
| 1-(tert-Butoxycarbonyl)-3-piperidone >98.0%(GC) | B3309 | 5g | $34 |
| 1-(tert-Butoxycarbonyl)-3-piperidone >98.0%(GC) | B3309 | 25g | $109 |
| N-Boc-3-piperidone Asreported | 261926 | 5g | $333 |
| More product size | |||
| Melting point | 35-40 °C (lit.) |
|---|---|
| Boiling point | 289.8±33.0 °C(Predicted) |
| Density | 1.099±0.06 g/cm3(Predicted) |
| Flash point | >230 °F |
| storage temp. | 2-8°C |
| pka | -1.71±0.20(Predicted) |
| form | Liquid |
| color | Clear colorless |
| Water Solubility | It is insoluble in water. |
| BRN | 5936353 |
| InChI | InChI=1S/C10H17NO3/c1-10(2,3)14-9(13)11-6-4-5-8(12)7-11/h4-7H2,1-3H3 |
| InChIKey | RIFXIGDBUBXKEI-UHFFFAOYSA-N |
| SMILES | N1(C(OC(C)(C)C)=O)CCCC(=O)C1 |
| CAS DataBase Reference | 98977-36-7(CAS DataBase Reference) |
| UNSPSC Code | 12352100 |
| NACRES | NA.22 |
SAFETY
Risk and Safety Statements
| Symbol(GHS) |  GHS07 |
|||||||||
|---|---|---|---|---|---|---|---|---|---|---|
| Signal word | Warning | |||||||||
| Hazard statements | H319-H315 | |||||||||
| Precautionary statements | P264-P280-P302+P352+P332+P313+P362+P364-P305+P351+P338+P337+P313-P305+P351+P338 | |||||||||
| PPE | Eyeshields, Gloves, type N95 (US) | |||||||||
| Safety Statements | 24/25 | |||||||||
| WGK Germany | 3 | |||||||||
| HazardClass | KEEP COLD | |||||||||
| HS Code | 29339900 | |||||||||
| Storage Class | 13 - Non Combustible Solids | |||||||||
| NFPA 704 |
|
1-Boc-3-piperidone price More Price(131)
| Manufacturer | Product number | Product description | CAS number | Packaging | Price | Updated | Buy |
|---|---|---|---|---|---|---|---|
| Sigma-Aldrich | 650811 | 1-Boc-3-piperidone 97% | 98977-36-7 | 25g | $80.7 | 2024-03-01 | Buy |
| Sigma-Aldrich | 650811 | 1-Boc-3-piperidone 97% | 98977-36-7 | 5g | $30 | 2023-06-20 | Buy |
| TCI Chemical | B3309 | 1-(tert-Butoxycarbonyl)-3-piperidone >98.0%(GC) | 98977-36-7 | 5g | $34 | 2026-04-30 | Buy |
| TCI Chemical | B3309 | 1-(tert-Butoxycarbonyl)-3-piperidone >98.0%(GC) | 98977-36-7 | 25g | $109 | 2026-04-30 | Buy |
| Usbiological | 261926 | N-Boc-3-piperidone Asreported | 98977-36-7 | 5g | $333 | 2026-06-03 | Buy |
1-Boc-3-piperidone Chemical Properties,Uses,Production
Chemical Properties
White to yellow low melting solid
Uses
1-Boc-3-piperidone, is used as an important raw material and intermediate used in organic Synthesis, pharmaceuticals, agrochemicals and dyestuff.
Synthesis
With 179g compound 3(1-BOC-3-piperidines alcohol) drop in the 2L reaction flask, drop into pimelinketone 1300g, aluminum isopropylate 88g, methylene dichloride 400ml is warming up to 80 ℃, insulation reaction 8h, reaction finishes to be cooled to room temperature, adds 10% sodium hydroxide 200ml, stirring at normal temperature 30min, filter, the filtrate normal pressure reclaims methylene dichloride, reclaim under reduced pressure pimelinketone again, reclaim finish after, add the 300ml dichloromethane extraction three times, it is dry concentrated to merge oil reservoir, gets 1-BOC-3-piperidone crude product.
Refining: with 1-BOC-3-piperidone crude product is that 60pa, temperature are to distill under 104 ~ 105 ℃ the condition at pressure, gets 1-BOC-3-piperidone elaboration 163g, 92.9%.
References
[1] Patent: CN107573278, 2018, A. Location in patent: Paragraph 0055; 0059-0061; 0076-0077
[2] Patent: US2011/105520, 2011, A1. Location in patent: Page/Page column 36
[3] Patent: WO2009/82134, 2009, A2. Location in patent: Page/Page column 37
[4] Patent: WO2013/13308, 2013, A1. Location in patent: Paragraph 00250-00252
[5] Patent: US2003/220341, 2003, A1. Location in patent: Page/Page column 15-16
1-Boc-3-piperidone Preparation Products And Raw materials
Raw materials
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Preparation Products
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| Supplier | Tel | Country | ProdList | Advantage | |
|---|---|---|---|---|---|
| Chongqing Ensky Pharmaceutical Co.,Ltd. | +86-86-2386815286 +8613983794297 | sales@ensky-chemical.com | China | 94 | 58 |
| Shanghai Quedan biology science and technology co., ltd | +86-13004146052 | lnzc@quedan.com.cn | China | 1022 | 58 |
| Zhengzhou Lingzhiyue Technology Co., Ltd | +86-0371-55074660 +86-13523716970 | Lingzhiyue@aliyun.com | China | 3145 | 58 |
| Anhui Yiao New Material Technology Co., Ltd | +86-18033737140 +86-17354101231 | sales1@hbganmiao.com | China | 227 | 58 |
| Xiamen Wonderful Bio Technology Co., Ltd. | +8613043004613 | Sara@xmwonderfulbio.com | China | 283 | 58 |
| Shandong Huisheng Import & Export Co., Ltd. | +86-13176845580 | da@zhongda-biotech.com | China | 232 | 58 |
| Anhui Zhongda Biotechnology Co., Ltd | +8619956560829 | justine@zhongda-biotech.com | China | 286 | 58 |
| Anhui Zhongda Biotechnology Co., Ltd | +8615689548120 | linda@zhongda-biotech.com | China | 193 | 58 |
| Anhui Ruihan Technology Co., Ltd | +8617756083858 | daisy@anhuiruihan.com | China | 973 | 58 |
| Hebei Ganmiao New material Technology Co., LTD | +86-17332992504 | sales8@hbganmiao.com | China | 300 | 58 |
Related articles
- Synthesis and Application of N-Boc-3-piperidone
- N-Boc-3-piperidone is an important pesticide, pharmaceutical intermediates and other chemical additives.
- Jul 20，2022
View Lastest Price from 1-Boc-3-piperidone manufacturers
| Image | Update time | Product | Price | Min. Order | Purity | Supply Ability | Manufacturer | |
|---|---|---|---|---|---|---|---|---|
 |
2024-08-20 | 1-Boc-3-Piperidinone
98977-36-7
|
$8.00-10.00 | 1kg | 99.9% | 20ton | Hebei Ganmiao New material Technology Co., LTD | |
 |
2024-06-11 | 1-Boc-3-piperidone
98977-36-7
|
1KG | 99% | 1 ton | Anhui Yiao New Material Technology Co., Ltd | ||
 |
2024-01-18 | 1-Boc-3-Piperidinone
98977-36-7
|
$88.00 | 1KG | 99% | 100000T | Xiamen Wonderful Bio Technology Co., Ltd. |
-
- 1-Boc-3-Piperidinone
98977-36-7
- $8.00-10.00
- 99.9%
- Hebei Ganmiao New material Technology Co., LTD
-
- 1-Boc-3-piperidone
98977-36-7
- $0.00
- 99%
- Anhui Yiao New Material Technology Co., Ltd
-
- 1-Boc-3-Piperidinone
98977-36-7
- $88.00
- 99%
- Xiamen Wonderful Bio Technology Co., Ltd.
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