4-ブロモ-1H-ピロロ[2,3-C]ピリジン
4-ブロモ-1H-ピロロ[2,3-C]ピリジン 物理性質
- 融點 :
- 188-189℃
- 沸點 :
- 337.6±22.0 °C(Predicted)
- 比重(密度) :
- 1.770
- 貯蔵溫度 :
- 2-8°C(protect from light)
- 酸解離定數(shù)(Pka):
- 13.73±0.40(Predicted)
- 外見 :
- solid
- 色:
- White to light brown
- InChI:
- InChI=1S/C7H5BrN2/c8-6-3-9-4-7-5(6)1-2-10-7/h1-4,10H
- InChIKey:
- NZUWATDXQMWXMY-UHFFFAOYSA-N
- SMILES:
- C1=NC=C(Br)C2C=CNC1=2
4-ブロモ-1H-ピロロ[2,3-C]ピリジン 価格
もっと(14)
| メーカー |
製品番號 |
製品説明 |
CAS番號 |
包裝 |
価格 |
更新時間 |
購入 |
|
富士フイルム和光純薬株式會社(wako)
|
W01COBOS-7901 |
4-ブロモ-1H-ピロロ[2,3-c]ピリジン
4-Bromo-1H-pyrrolo[2,3-c]pyridine |
69872-17-9 |
25g |
￥202500 |
2024-03-01 |
購入 |
|
富士フイルム和光純薬株式會社(wako)
|
W01COBOS-7901 |
4-Bromo-1H-pyrrolo[2,3-c]pyridine |
69872-17-9 |
25g×4 |
￥810000 |
2024-03-01 |
購入 |
|
富士フイルム和光純薬株式會社(wako)
|
W01APOOR55212 |
4-Bromo-6-azaindole |
69872-17-9 |
1g |
￥12500 |
2024-03-01 |
購入 |
|
富士フイルム和光純薬株式會社(wako)
|
W01COBOS-7901 |
4-ブロモ-1H-ピロロ[2,3-c]ピリジン
4-Bromo-1H-pyrrolo[2,3-c]pyridine |
69872-17-9 |
1g |
￥14500 |
2024-03-01 |
購入 |
|
富士フイルム和光純薬株式會社(wako)
|
W01COBOS-7901 |
4-ブロモ-1H-ピロロ[2,3-c]ピリジン
4-Bromo-1H-pyrrolo[2,3-c]pyridine |
69872-17-9 |
5g |
￥47500 |
2024-03-01 |
購入 |
4-ブロモ-1H-ピロロ[2,3-C]ピリジン 化學特性,用途語,生産方法
合成
2-(3-bromo-5-nitropyridin-4-yl)-N, N-dimethylethylenamine (2.38 g, 8.78 mmol) and iron powder (~325 mesh, 2.45 g, 43.9 mmol) were stirred in acetic acid (25 mL). The red mixture was heated to reflux and turned grayish-green with a white precipitate. After refluxing for 45 min, the reaction was cooled, diluted with EtOAc (150 mL), filtered through Celite and rinsed with additional EtOAc. The filtrate was slowly basified to pH 8 with saturated aqueous NaHCO3, and the aqueous layer was extracted with EtOAc. The combined organics were washed with brine, dried (MgSO4), filtered, and concentrated in vacuo. Silica gel chromatography (eluding with 5% MeOH in EtOAc) afforded 4-bromo-1H-pyrrolo[2,3-c]pyridine (1.26 g, 73%) as a yellow solid.
4-ブロモ-1H-ピロロ[2,3-C]ピリジン 上流と下流の製品情報
原材料
準備製品
4-ブロモ-1H-ピロロ[2,3-C]ピリジン 生産企業(yè)
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4-ブロモ-1H-ピロロ[2,3-C]ピリジン スペクトルデータ(1HNMR)
69872-17-9(4-ブロモ-1H-ピロロ[2,3-C]ピリジン)キーワード:
- 69872-17-9
- 4-bromo-1H-pyrrolo[2,3-c]pyridine
- 1H-PYRROLO[2,3-C]-PYRIDINE,4-BROMO-
- 4-BroM-6-azaindol
- 4-broMo-1H-pyrrolo[2,3-c]pyridin
- 4-Bromo-6-azaindole 97%
- 4-Bromo-1H-pyrrolo[2,3-c]pyridine (69872-17-9)
- 4-Bromo-6-azaindole
- 4-ブロモ-1H-ピロロ[2,3-C]ピリジン