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(Trimethylsilyl)methylamine

(Trimethylsilyl)methylamine ??? ???

?? ??:: 18166-02-4

???:: (Trimethylsilyl)methylamine

???(??):: (trimethylsilyl)methanamine;AMTMS;rimethylsilylmethanamine;Trimethylsilylmethaneamine;(TRIMETHYLSILYL)METHYLAMINE;2-AMINOMETHYLTRIMETHYLSILANE;(AMINOMETHYL)TRIMETHYLSILANE;1-(trimethylsilyl)methylamine;Methanamine, 1-(trimethylsilyl)-;Methylamine, 1-(trimethylsilyl)-,

CBNumber:: CB1158779

???:: C4H13NSi

??? ??:: 103.24

MOL ??:: 18166-02-4.mol

MSDS ??:: SDS

?? ?? 105

(Trimethylsilyl)methylamine ??

???: <0°C

?? ?: 92-94 °C(lit.)

??: 0.771 g/mL at 20 °C(lit.)

???: n20/D 1.416

???: 9°C

?? ??: Keep in dark place,Inert atmosphere,Room temperature

?? ?? (pKa): 10.89±0.10(Predicted)

??? ??: liquid

Specific Gravity: 0.7697

Hydrolytic Sensitivity: 4: no reaction with water under neutral conditions

BRN: 1731488

InChI: InChI=1S/C4H13NSi/c1-6(2,3)4-5/h4-5H2,1-3H3

InChIKey: YVWPNDBYAAEZBF-UHFFFAOYSA-N

SMILES: C([Si](C)(C)C)N

CAS ??????: 18166-02-4(CAS DataBase Reference)

NIST: Trimethylsilylmethylamine(18166-02-4)

?? ? ?? ??
?? ? ???? ?? (GHS)

??? ??	F,C
?? ???? ??	11-34-37
?????	16-26-36/37/39-45
????(UN No.)	UN 2733 3/PG 2
WGK ??	3
F ??????	3-10
TSCA	No
?? ??	3.1
????	II
???? ???	3 - Flammable liquids
Hazard Classifications	Flam. Liq. 2 Skin Corr. 1B

????(GHS):

?? ?:

Danger

??·?? ??:

??	??·?? ??	?? ??	??	?? ?	?? ??	P- ??
H225	???? ?? ? ??	??? ??	?? 2	??		P210,P233, P240, P241, P242, P243,P280, P303+ P361+P353, P370+P378,P403+P235, P501
H314	??? ?? ??? ?? ??? ???	????? ?? ?????	?? 1A, B, C	??		P260,P264, P280, P301+P330+ P331,P303+P361+P353, P363, P304+P340,P310, P321, P305+ P351+P338, P405,P501

??????:

P210	?·???·??·????? ????? - ?? ???.
P233	??? ??? ?????. ??? ??? ? ?? ?? ??? ???? ?????.
P240	??? ????? ?? ? ??????.
P280	????/???/???/?????? ?????.
P303+P361+P353	??(?? ????)? ??? ??? ?? ??? ??? ????? ??? ?? ????/?????.
P305+P351+P338	?? ??? ? ?? ?? ???? ????. ???? ?????? ?????. ?? ????.

(Trimethylsilyl)methylamine C??? ??, ??, ??

Purification Methods

A possible contaminant is hexamethyldisiloxane. It should have two 1H NMR signals in CDCl3; if not, dissolve it in *C6H6, shake it with 15% aqueous KOH, separate, dry (Na2SO4), filter, evaporate and distil it using a still of ca 10 theoretical plates. The water azeotrope has b 83o/735mm; hence it is important to dry the extract well. The hydrochloride has m 198-199o (from MeOH or Me2CO). [Noll et al. J Am Chem Soc 73 3867 1951, Beilstein 4 IV 3878.]

(Trimethylsilyl)methylamine ?? ?? ? ???

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(TRIMETHYLSILYL)DIAZOMETHANE

(Trimethylsilyl)methylamine ?? ??

???( 105)?? ??

???	??	???	??	?? ?	??
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(Trimethylsilyl)methylamine ?? ??:

?????? ????????? ????????? ???????(??????) ?????????? ???????? ??? ?? ??????????? ????????? (?? ???? ??) ???? ?? ????????? ???? 1-((??(4-??????)????)??)-1H-1,2,4-???? ?? ?? ? ?? ? N-[(??????)??]??? trimethylamine oxide N-(Trimethylsilyl)acetamide N-[(Trimethylsilyl)methyl]benzylamine TRIMETHYLSILYLMETHYL AZIDE

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