3-(4-BROMOPHENOXY)PROPANOIC ACID synthesis
- Product Name:3-(4-BROMOPHENOXY)PROPANOIC ACID
- CAS Number:93670-18-9
- Molecular formula:C9H9BrO3
- Molecular Weight:245.07
7170-38-9
174 suppliers
$8.00/1g
93670-18-9
59 suppliers
$76.00/1g
Yield:93670-18-9 98%
Reaction Conditions:
with N-Bromosuccinimide;sodium hydroxide in water at 20; for 1 h;
Steps:
8
Keep at room temperature, compound III (152 g, 0.9 mole) and sodium hydroxide (80 g, 2 mole) in 1.5 liters of solution added in batches in NBS (178 g, 1 mole). After dropping stirring 1 hour. For concentrated hydrochloric acid to adjust the pH to 2 - 3. Collecting the solid and dry it. The product 218 g (98%).
References:
CN106699716,2017,A Location in patent:Paragraph 0020; 0033
57-57-8
177 suppliers
$24.73/250mgs:
106-41-2
497 suppliers
$13.00/5g
93670-18-9
59 suppliers
$76.00/1g
106-41-2
497 suppliers
$13.00/5g
93670-18-9
59 suppliers
$76.00/1g