4-HYDROXY-2'-METHYLDIPHENYLAMINE synthesis
4synthesis methods
- Product Name:4-HYDROXY-2'-METHYLDIPHENYLAMINE
- CAS Number:23197-53-7
- Molecular formula:C13H13NO
- Molecular Weight:199.25
Yield:23197-53-7 92%
Reaction Conditions:
with chloro[2-(dicyclohexylphosphino)-3,6-dimethoxy-2',4',6'-triisopropyl-1,1'-biphenyl][2-(2-aminoethyl)phenyl]palladium(ll);potassium carbonate in tert-butyl alcohol at 110; for 24 h;Inert atmosphere;
References:
Maiti, Debabrata;Buchwald, Stephen L. [Journal of the American Chemical Society,2009,vol. 131,# 47,p. 17423 - 17429] Location in patent:supporting information; experimental part
