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638-73-3

chlorodiiodomethane synthesis

5synthesis methods
The preparative methods of chlorodiiodomethane: reaction of Iodoform with Mercury(II) Chloride; reaction of Chloroform with Ethyl Iodide in the presence of Aluminum Chloride; reaction of chloroform with Sodium  Iodide and Sodium Hydroxide under phase transfer catalysis[1-2]. 
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Yield:638-73-3 30% ,594-04-7 1% ,75-11-6 1%

Reaction Conditions:

with mercury dichloride at 130; for 2 h;Title compound not separated from byproducts;Substitution;

References:

Cancho, Beatriz;Ventura, Francesc;Galceran, Materesa;Diaz, Alfredo;Ricart, Susagna [Water Research,2000,vol. 34,# 13,p. 3380 - 3390]

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