4-(甲基磺?；?苯肼鹽酸鹽
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- CAS號:
- 17852-67-4
- 英文名:
- 4-(Methylsulfonyl)phenylhydrazine hydrochloride
- 英文別名:
- TIMTEC-BB SBB003335;4-Hydrazino-1-(methylsulphonyl)benzene;4-METHYLSULPHONYLPHENYLHYDRAZINE HYDROCHLORIDE;4-(Methylsulfonyl)phenylhydrazine hydrochloride;5-(4-methylsulfonylphenyl)-2-furancarboxylic acid;(4-Methanesulfonyl-phenyl)-hydrazine hydrochloride;4-(Methylsulfonyl)phenylhydrazine hydrochloride,95%;4-Hydrazino-1-(methylsulfonyl)benzene hydrochloride;4-Hydrazino-1-(methylsulphonyl)benzene hydrochloride;4-(Methylsulfonyl)phenylhydrazine hydrochloride, 95% 2.5GR
- 中文名:
- 4-(甲基磺?；?苯肼鹽酸鹽
- 中文別名:
- 4-甲砜基苯肼鹽酸鹽;4-甲基磺酰苯肼鹽酸鹽;4-(甲基磺酰基)苯肼鹽酸鹽;1-(4-(甲磺?；?苯基)肼鹽酸鹽
- CBNumber:
- CB4273462
- 分子式:
- C7H11ClN2O2S
- 分子量:
- 222.69
- MOL File:
- 17852-67-4.mol
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4-(甲基磺酰基)苯肼鹽酸鹽化學(xué)性質(zhì)
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熔點:
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202 °C
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儲存條件:
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under inert gas (nitrogen or Argon) at 2-8°C
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形態(tài):
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Crystalline Powder
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顏色:
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Off-white to light yellow
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水溶解性:
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SOLUBLE
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4-(甲基磺酰基)苯肼鹽酸鹽性質(zhì)、用途與生產(chǎn)工藝
生產(chǎn)方法
以4-甲磺?；桨窞樵虾铣?-(甲基磺酰基)苯肼鹽酸鹽的一般步驟：將100 mL鹽酸加入500 mL四頸燒瓶中，通過冰水浴將燒瓶內(nèi)溫度冷卻至-10℃或更低，并確保溫度不超過-10℃。隨后，加入并溶解10.27 g（0.06 mol）4-(甲基磺酰基)苯胺。待放熱反應(yīng)停止后，在保持燒瓶溫度低于-10℃的條件下，緩慢加入4.47 g（0.065 mol）亞硝酸鈉，并在1小時內(nèi)滴加30 g蒸餾水。滴加完畢后，繼續(xù)在1小時內(nèi)滴加67.7 g（0.30 mol）氯化錫二水合物溶于60 mL鹽酸的溶液，同時嚴(yán)格控制反應(yīng)溫度在-10℃或更低。反應(yīng)完成后，過濾收集固體產(chǎn)物，并在60℃下使用真空干燥器干燥12小時，得到4-(甲基磺?；?苯肼鹽酸鹽（中間體G1）。該步驟基于4-(甲基磺?；?苯胺的收率為67.9 mol%。
參考文獻：
[1] Patent: JP2018/95798, 2018, A. Location in patent: Paragraph 0081; 0084
4-(甲基磺?；?苯肼鹽酸鹽
上下游產(chǎn)品信息
上游原料
下游產(chǎn)品
| 更新日期 | 產(chǎn)品編號 | 產(chǎn)品名稱 | CAS編號 | 包裝 | 價格 |
|---|
| 2026/07/06 | 42496 | 4-(甲基磺酰基)苯肼鹽酸鹽
4-(Methylsulfonyl)phenylhydrazine Hydrochloride, 95%, Thermo Scientific Chemicals | 17852-67-4 | 2.5g | 1373元 |
| 2026/06/05 | XW178526741 | 4-(甲基磺?；?苯肼鹽酸鹽
4-(Methylsulfonyl)phenylhydrazine hydrochloride | 17852-67-4 | 2.5g | 1209元 |
4-(甲基磺?；?苯肼鹽酸鹽
生產(chǎn)廠家
17852-67-4, 4-(甲基磺酰基)苯肼鹽酸鹽 相關(guān)搜索:
- C7H10N2O2SHCl
- 4-(甲基磺?；?苯肼鹽酸鹽
- 4-甲基磺酰苯肼鹽酸鹽
- 1-(4-(甲磺?；?苯基)肼鹽酸鹽
- 4-甲砜基苯肼鹽酸鹽
- 17852-67-4
- (4-(Methylsulfonyl)phenyl)hydrazine hydrochloride - [M46468]
- Hydrazine, [4-(methylsulfonyl)phenyl]-, hydrochloride (1:1)
- 5-(4-methylsulfonylphenyl)-2-furancarboxylic acid
- 4-Hydrazino-1-(methylsulfonyl)benzene hydrochloride
- 1-Hydrazino-4-(methylsulphonyl)benzene hydrochloride, 4-Hydrazinophenyl methyl sulphone hydrochloride
- (4-Methanesulfonyl-phenyl)-hydrazine hydrochloride
- 4-(Methylsulfonyl)phenylhydrazine hydrochloride, 95% 2.5GR
- 4-Hydrazino-1-(methylsulphonyl)benzene hydrochloride
- 4-Hydrazino-1-(methylsulphonyl)benzene
- 4-(Methylsulfonyl)phenylhydrazine hydrochloride
- 4-(Methylsulfonyl)phenylhydrazine hydrochloride,95%
- TIMTEC-BB SBB003335
- 4-METHYLSULPHONYLPHENYLHYDRAZINE HYDROCHLORIDE