N-chloro-N-cyclohexylbenzenesulfonaMide Chemische Eigenschaften,Einsatz,Produktion Methoden
Verwenden
N-chloro-N-cyclohexylbenzenesulfonaMide is used for radical chlorination at allylic or benzylic carbon.
Synthese
Synthesis of N-chloro-N-cyclohexylbenzenesulfonaMide:N-chloro-N-cyclohexylbenzenesulfonaMide is N-cyclohexylbenzenesulfonamide can be prepared by addition of benzenesulfonyl chloride to a solution of cyclohexylamine in pyridine and purified by recrystallization from ethanol. N-Chlorination is accomplished by treating a solution of N-cyclohexylbenzenesulfonamide in dichloromethane with NaOCl solution at 0 °C followed by dropwise addition of glacial acetic acid.
Lager
Store under nitrogen in the dark. This toxic reagent should be handled in a fume hood.
N-chloro-N-cyclohexylbenzenesulfonaMide Upstream-Materialien And Downstream Produkte
Upstream-Materialien
Downstream Produkte
