(3-Bromophenyl)triphenylsilane
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- CAS-Nr.
- 185626-73-7
- Englisch Name:
- (3-Bromophenyl)triphenylsilane
- Synonyma:
- 3-Bromotetraphenylsilane;(3-Bromophenyl)triphenylsilane;(3-Bromopheny|) tripheny|si|ane;Silane, (3-bromophenyl)triphenyl-;1-bromo-3-(triphenylsilyl)-Benzene;3-bromophenyltriphenylsilyl chloride;Benzene, 1-bromo-3-(triphenylsilyl)-;(3-bromophenyl)triphenylsiliconalkane;(3-Bromophenyl)triphenylsilane - [B89405]
- CBNumber:
- CB02973311
- Summenformel:
- C24H19BrSi
- Molgewicht:
- 415.4
- MOL-Datei:
- 185626-73-7.mol
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(3-Bromophenyl)triphenylsilane Eigenschaften
- Schmelzpunkt:
- 135.0 to 139.0 °C
- Siedepunkt:
- 469.9±37.0 °C(Predicted)
- Dichte
- 1.30±0.1 g/cm3(Predicted)
- storage temp.
- Sealed in dry,Room Temperature
- Aggregatzustand
- powder to crystal
- Farbe
- White to Light yellow
- InChI
- InChI=1S/C24H19BrSi/c25-20-11-10-18-24(19-20)26(21-12-4-1-5-13-21,22-14-6-2-7-15-22)23-16-8-3-9-17-23/h1-19H
- InChIKey
- WTYKIOBQNRWDQP-UHFFFAOYSA-N
- SMILES
- C1(Br)=CC=CC([Si](C2=CC=CC=C2)(C2=CC=CC=C2)C2=CC=CC=C2)=C1
- CAS Datenbank
- 185626-73-7
(3-Bromophenyl)triphenylsilane Chemische Eigenschaften,Einsatz,Produktion Methoden
Verwenden
(3-Bromophenyl)triphenylsilane is used as a material for organic electroluminescent elements, display devices and lighting devices.
Synthese
1,3-Dibromobenzene 20 g (84.77 mmol) was dissolved in THF 500 mL and then cooled to a temperature of -78. n-BuLi 2.5M 33.9 mL(84.77 mmol) was slowly added thereinto and then stirred at a temperature of -78 for 1 hour. Chlorotriphenylsilane ((C6H5)3SiCl) 29.9 g was dissolved in THF 100 mL, and this solution was added to the above reaction mixture. The resultant mixture was slowly warmed to room temperature and stirred for 12 hours. Then, extraction with EA, wash with distilled water and aqueous NaCl solution, drying over MgSO4, distillation under reduced pressure, and recrystallization with MC-MeOH in the ratio of 1:10, were sequentially performed, thereby obtaining (3-Bromophenyl)triphenylsilane 18 g(95 percent).
(3-Bromophenyl)triphenylsilane Upstream-Materialien And Downstream Produkte
Upstream-Materialien
Downstream Produkte
(3-Bromophenyl)triphenylsilane Anbieter Lieferant Produzent Hersteller Vertrieb H?ndler.
Global( 123)Lieferanten
185626-73-7()Verwandte Suche:
- (3-Bromophenyl)triphenylsilane
- Silane, (3-bromophenyl)triphenyl-
- 3-bromophenyltriphenylsilyl chloride
- 3-Bromotetraphenylsilane
- Benzene, 1-bromo-3-(triphenylsilyl)-
- 1-bromo-3-(triphenylsilyl)-Benzene
- (3-Bromophenyl)triphenylsilane - [B89405]
- (3-Bromopheny|) tripheny|si|ane
- (3-bromophenyl)triphenylsiliconalkane
- 185626-73-7
