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Methanesulfenic acid chloride

Methanesulfenic acid chloride Struktur
5813-48-9
CAS-Nr.
5813-48-9
Englisch Name:
Methanesulfenic acid chloride
Synonyma:
Methanesulfenyl chloride;Methylthio chloride;Methylsulfur monochloride;Methanesulfenic acid chloride;Methanesulfenyl chloride (6CI,7CI,8CI,9CI)
CBNumber:
CB22135911
Summenformel:
CH3ClS
Molgewicht:
82.55
MOL-Datei:
5813-48-9.mol

Methanesulfenic acid chloride Eigenschaften

Siedepunkt:
27-28 °C(Press: 53-60 Torr)
Dichte
1.172±0.06 g/cm3(Predicted)
L?slichkeit
sol ether, THF, dichloromethane, chloroform, carbon tetrachloride, dimethoxyethane

Sicherheit

Methanesulfenic acid chloride Chemische Eigenschaften,Einsatz,Produktion Methoden

Verwenden

Methanesulfenic acid chloride reacts as a pseudohalogen; reacts with carbanions and enolates to add the thiomethyl group α to the carbonyl; adds across the double bonds of alkenes and allenes; adds across triple bond of alkynes.

synthetische

To a flask containing 23.6 gm (0.25 mole) of dimethyl disulfide at - 1 5 ° to -20°C is slowly added dropwise 34 gm (0.25 mole) of freshly distilled sulfuryl chloride while keeping the temperature at -15° to -20°C. The reaction mixture is stirred for 1 hr, and then distilled to afford 37.1 gm (90%), b.p. 27-28°C (53-60 mm Hg); NMR, 2.91 ppm (singlet). The crude product can also be used without distillation since most of the material is product.
Preparation of Methanesulfenyl Chloride

Lager

Methanesulfenic acid chloride undergoes decomposition within 1-2 d even when kept in a refrigerator; lasts less than 1 month when stored at -78 °C.

l?uterung methode

Methanesulfenic acid chloride can be used crude from the above preparations. If purification is necessary it must be distilled at low temperature, under vacuum, due to its instability.

Methanesulfenic acid chloride Upstream-Materialien And Downstream Produkte

Upstream-Materialien

Downstream Produkte


Methanesulfenic acid chloride Anbieter Lieferant Produzent Hersteller Vertrieb H?ndler.

Global( 1)Lieferanten
Firmenname Telefon E-Mail Land Produktkatalog Edge Rate
Shaanxi Didu New Materials Co. Ltd
+86-86-17392712779 +8617792793228
1069@dideu.com China 8661 58

  • Methanesulfenic acid chloride
  • Methylsulfur monochloride
  • Methylthio chloride
  • Methanesulfenyl chloride (6CI,7CI,8CI,9CI)
  • Methanesulfenyl chloride
  • 5813-48-9
  • CH3ClS
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