D-erythro-Pentonic acid, 2-deoxy-4-C-ethynyl-, γ-lactone, 3,5-bis(4-methylbenzoate) Chemische Eigenschaften,Einsatz,Produktion Methoden

Synthese

D-erythro-Pentonic acid, 2-deoxy-4-C-ethynyl-, γ-lactone, 3,5-bis(4-methylbenzoate) is synthesised by reacting D-erythro-Pentonic acid, 2-deoxy-4-C-ethynyl-, γ-lactone with 4-Methylbenzoyl chloride in a pyridine solution. Yield: 95%. The specific reaction process and steps are as follows^[1]:
(1) Add toluoyl chloride (15.2 g) to a solution of (4S,5R)-5-ethynyl-4-hydroxy-5-(hydroxymethyl)dihydrofuran-2(3H)-one (7.5 g) in pyridine (38 mL) at 0 °C.
(2) Stir the resulting mixture for 2 hours at 0 °C.
(3) Add water (45 mL) slowly at 0-5 °C, causing the product to crystallize.
(4) Filter the reaction mixture.
(5) Wash the filter cake with ice water.
(6) Dry the product.

D-erythro-Pentonic acid, 2-deoxy-4-C-ethynyl-, γ-lactone, 3,5-bis(4-methylbenzoate) Upstream-Materialien And Downstream Produkte

Upstream-Materialien

Downstream Produkte

D-erythro-Pentonic acid, 2-deoxy-4-C-ethynyl-, γ-lactone, 3,5-bis(4-methylbenzoate) Anbieter Lieferant Produzent Hersteller Vertrieb H?ndler.

Firmenname	Telefon	E-Mail	Land	Produktkatalog	Edge Rate
Jinan Carbotang Biotech Co.,Ltd.	+8615866703830	figo.gao@foxmail.com	China	8497	58
Unibest Industrial Co.,Ltd.	+86-0574-27855777 +8618758850676	info@unibestcn.com	China	271	58
Shanghai Boc Chemical Co.,Ltd	021-34975603-808 18721111801	sales@bocpharma.com	China	994	64

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• D-erythro-Pentonic acid, 2-deoxy-4-C-ethynyl-, γ-lactone, 3,5-bis(4-methylbenzoate)
• 2072080-27-2