2-(4-bromophenyl)-4,6-diphenyl-1,3,5-triazine
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- CAS-Nr.
- 23449-08-3
- Englisch Name:
- 2-(4-bromophenyl)-4,6-diphenyl-1,3,5-triazine
- Synonyma:
- PTZ-Br;)-4,6-diphenyL;2-(4-bromophenyl)-4;1,3,5-Triazine, 2-(4-bromopheny)-4,6-dipheny-;：2-(4-broMophenyl)-4,6-diphenyl-1,3,5-Triazin;2-(4-bromophenyl)-4,6-diphenyl-1,3,5-triazine;1,3,5-Triazine, 2-(4-broMophenyl)-4,6-diphenyl-;23449-08-3 1,3,5-Triazine, 2-(4-bromophenyl)-4,6-diphenyl-
- CBNumber:
- CB32073270
- Summenformel:
- C21H14BrN3
- Molgewicht:
- 388.26
- MOL-Datei:
- 23449-08-3.mol
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2-(4-bromophenyl)-4,6-diphenyl-1,3,5-triazine Eigenschaften
- Schmelzpunkt:
- 200.0 to 204.0 °C
- Siedepunkt:
- 573.9±52.0 °C(Predicted)
- Dichte
- 1.381
- storage temp.
- Sealed in dry,Room Temperature
- Aggregatzustand
- powder to crystal
- pka
- 0.45±0.10(Predicted)
- Farbe
- White to Almost white
- InChI
- InChI=1S/C21H14BrN3/c22-18-13-11-17(12-14-18)21-24-19(15-7-3-1-4-8-15)23-20(25-21)16-9-5-2-6-10-16/h1-14H
- InChIKey
- AYHGAQGOMUQMTR-UHFFFAOYSA-N
- SMILES
- N1=C(C2=CC=CC=C2)N=C(C2=CC=CC=C2)N=C1C1=CC=C(Br)C=C1
2-(4-bromophenyl)-4,6-diphenyl-1,3,5-triazine Chemische Eigenschaften,Einsatz,Produktion Methoden
Chemische Eigenschaften
white solid powder
Synthese
The compound, 2-chloro-4,6-diphenyl-1,3,5-triazine (50 g, 187 mmol) was dissolved in THF (1 L) under a nitrogen environment, (4-bromophenyl)boronic acid (45 g, 224.12 mmol, Aldrich Corporation), and tetrakis(triphenylphosphine)palladium (2.1 g, 1.87 mmol) were added thereto, and the mixture was stirred. Potassium carbonate saturated in water (64 g, 467 mmol) was added thereto, and the obtained mixture was heated and refluxed at 80° C. for 12 hours. When the reaction was complete, water was added to the reaction solution, and the mixture was extracted with dichloromethane (DCM) and then, filtered after removing moisture with anhydrous MgSO4 and concentrated under a reduced pressure. This obtained residue was separated and purified through flash column chromatography to obtain 2-(4-bromophenyl)-4,6-diphenyl-1,3,5-triazine (70 g and 96%).
2-(4-bromophenyl)-4,6-diphenyl-1,3,5-triazine Upstream-Materialien And Downstream Produkte
Upstream-Materialien
2-chloro-4,6-diphenyl-1,3,5-triazine
2-iodo-4,6-diphenyl-1,3,5-triazine
Benzamidiniumchlorid
Benzonitril
4-Brombenzoylchlorid
4-Brombenzaldehyd
2-(4-BROMO-PHENYL)-4,4,5,5-TETRAMETHYL-[1,3,2]DIOXABOROLANE
Tetrahydrofuran
Kaliumcarbonat
Dihydroxy-4-bromphenylboran
Downstream Produkte
2-(4-bromophenyl)-4,6-diphenyl-1,3,5-triazine Anbieter Lieferant Produzent Hersteller Vertrieb H?ndler.
Global( 224)Lieferanten
23449-08-3()Verwandte Suche:
- 2-(4-bromophenyl)-4,6-diphenyl-1,3,5-triazine
- 1,3,5-Triazine, 2-(4-broMophenyl)-4,6-diphenyl-
- PTZ-Br
- )-4,6-diphenyL
- 1,3,5-Triazine, 2-(4-bromopheny)-4,6-dipheny-
- 2-(4-bromophenyl)-4
- 23449-08-3 1,3,5-Triazine, 2-(4-bromophenyl)-4,6-diphenyl-
- ：2-(4-broMophenyl)-4,6-diphenyl-1,3,5-Triazin
- 23449-08-3
- 23449-8-3
- 14367-46-7
- 1,3,5-triazine
- oled intermediate
- 23449-08-3
- OLED
