[6aS,(+)]-9α-Ethenyl-2,6,6aα,7,8,9,10,10aβ-octahydro-10α-isocyano-6,6,9-trimethylnaphtho[1,2,3-cd]indole Chemische Eigenschaften,Einsatz,Produktion Methoden

synthetische

To a cooled ( 20 C°) solution of the formamide (6.5 mg) in pyridine (0.4 mL) under Ar atmosphere was added phosphoryl chloride (11 mL) and the mixture was stirred at the same temperature for 40 min. Addition of saturated aq. NaHCO3, extraction with 10% MeOH/ CH2Cl2, standard work-up, and PTLC (hexane/EtOAc, 4:1) afforded (±)-hapalindole U 1629 (4.5 mg, 73%) as colorless needles; mp 240–242 C° (CH2Cl2/hexane).
During the synthesis and evaluation of a series of arachidonate epoxy inhibitors, 1631 was prepared in 85% yield by dehydration of the formamide 1630 with phosphoryl chloride.

[6aS,(+)]-9α-Ethenyl-2,6,6aα,7,8,9,10,10aβ-octahydro-10α-isocyano-6,6,9-trimethylnaphtho[1,2,3-cd]indole Upstream-Materialien And Downstream Produkte

Upstream-Materialien

Downstream Produkte

[6aS,(+)]-9α-Ethenyl-2,6,6aα,7,8,9,10,10aβ-octahydro-10α-isocyano-6,6,9-trimethylnaphtho[1,2,3-cd]indole Anbieter Lieferant Produzent Hersteller Vertrieb H?ndler.

Firmenname	Telefon	E-Mail	Land	Produktkatalog	Edge Rate

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• [6aS,(+)]-9α-Ethenyl-2,6,6aα,7,8,9,10,10aβ-octahydro-10α-isocyano-6,6,9-trimethylnaphth[1,2,3-cd]indole
• [6aS,(+)]-9α-Ethenyl-2,6,6aα,7,8,9,10,10aβ-octahydro-10α-isocyano-6,6,9-trimethylnaphtho[1,2,3-cd]indole
• Dechlorohapalindol A-10a-epimer
• Hapalindole U
• 106928-30-7