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9-Phenylanthracen

9-phenylanthracene Struktur
602-55-1
CAS-Nr.
602-55-1
Bezeichnung:
9-Phenylanthracen
Englisch Name:
9-phenylanthracene
Synonyma:
NSC 90796;9-phenylantracene;9-PHENYLANTHRACENE;Phenylanthracene,98%;anthracene,9-phenyl-;9-Phenylanthracene97%;9-Phenylanthracene>9-phenylanthracene-D9;9-Phenylanthracene,98%;9-Phenylanthracene 97%
CBNumber:
CB8778824
Summenformel:
C20H14
Molgewicht:
254.33
MOL-Datei:
602-55-1.mol

9-Phenylanthracen Eigenschaften

Schmelzpunkt:
153-155 °C (lit.)
Siedepunkt:
417 °C (lit.)
Dichte
1.1180 (estimate)
Brechungsindex
1.7040 (estimate)
storage temp. 
Sealed in dry,Room Temperature
L?slichkeit
Chloroform (Slightly), Ethyl Acetate (Slightly)
Aggregatzustand
Solid
Farbe
Off-white to pale brown
Sensitive 
Light Sensitive
BRN 
1910570
InChI
InChI=1S/C20H14/c1-2-8-15(9-3-1)20-18-12-6-4-10-16(18)14-17-11-5-7-13-19(17)20/h1-14H
InChIKey
LUBXLGUQZVKOFP-UHFFFAOYSA-N
SMILES
C1=C2C(C=C3C(=C2C2=CC=CC=C2)C=CC=C3)=CC=C1
CAS Datenbank
602-55-1(CAS DataBase Reference)
EPA chemische Informationen
Anthracene, 9-phenyl- (602-55-1)
Sicherheit
  • Risiko- und Sicherheitserkl?rung
  • Gefahreninformationscode (GHS)
Kennzeichnung gef?hrlicher N
R-S?tze: 50/53
S-S?tze: 60-61
RIDADR  UN 3077 9/PG 3
WGK Germany  3
HazardClass  9
HS Code  29029090
Speicherklasse 11 - Combustible Solids
Hazard Classifications Aquatic Acute 1
Aquatic Chronic 1
Bildanzeige (GHS) Environment (GHS09)
Alarmwort Warnung
Gefahrenhinweise
Code Gefahrenhinweise Gefahrenklasse Abteilung Alarmwort Symbol P-Code
H410 Sehr giftig für Wasserorganismen mit langfristiger Wirkung. Langfristig (chronisch) gew?ssergef?hrdend Kategorie 1 Warnung P273, P391, P501
Sicherheit
P273 Freisetzung in die Umwelt vermeiden.
P501 Inhalt/Beh?lter ... (Entsorgungsvorschriften vom Hersteller anzugeben) zuführen.

9-Phenylanthracen Chemische Eigenschaften,Einsatz,Produktion Methoden

R-S?tze Betriebsanweisung:

R50/53:Sehr giftig für Wasserorganismen, kann in Gew?ssern l?ngerfristig sch?dliche Wirkungen haben.

S-S?tze Betriebsanweisung:

S60:Dieses Produkt und sein Beh?lter sind als gef?hrlicher Abfall zu entsorgen.
S61:Freisetzung in die Umwelt vermeiden. Besondere Anweisungen einholen/Sicherheitsdatenblatt zu Rate ziehen.

Chemische Eigenschaften

Pale Yellow Plates

Verwenden

9-Phenylanthracene is used to synthesize organic light-emitting material intermediates.

synthetische

The synthesis of 9-phenylanthracene involved mixing phenylboronic acid (2.13 g, 17.49 mmol), 9-bromoanthracene (3 g, 11.66 mmol), Pd(PPh3)4 (140 mg, 0.12 mmol), K2CO3 (16 mL, 2 M), and ethanol (8 mL) in a 100 mL flask with anhydrous toluene (32 mL). The mixture was refluxed for 48 h under nitrogen. After cooled to room temperature, the reaction mixture was quenched with dilute hydrochloric acid solution and extracted with CH2Cl2. The organic extracts were dried over anhydrous MgSO4 and concentrated by rotary evaporation. The crude product was further purified by silica gel column chromatography (CH2Cl2/petroleum ether (1:4,v/v)) to get a white powder (2.43 g, 81.9 %). 1H NMR (500 MHz, CDCl3) δ 8.53 (s, 1H), 8.08 (d, J = 8.5 Hz, 2H), 7.70 – 7.67 (m, 2H), 7.63 – 7.54 (m, 3H), 7.50 – 7.45 (m, 4H), 7.37 (ddd, J = 8.7, 6.5, 1.2 Hz, 2H). EI-MS (m/z): Calculated for C20H14: 254.33. Found [M+]: 253.02.
preparation of 9-phenylanthracene
Synthesis of 9-phenylanthracene

l?uterung methode

Chromatograph it on alumina in *C6H6 and recrystallise it from AcOH or toluene. [Beilstein 5 H 725, 5 II 639, 5 III 2462.]

9-Phenylanthracen Upstream-Materialien And Downstream Produkte

Upstream-Materialien

Downstream Produkte


9-Phenylanthracen Anbieter Lieferant Produzent Hersteller Vertrieb H?ndler.

Global( 194)Lieferanten
Firmenname Telefon E-Mail Land Produktkatalog Edge Rate
Hebei Xinsheng New Material Technology Co., LTD.
+86-16632316109
xinshengkeji@xsmaterial.com China 1085 58
HANGZHOU HAILAN CHEMICAL CO.,LTD.
+86-57156122185 +86-15967590394
sales@hailan-chem.com China 2994 58
Springchem New Material Technology Co.,Limited
+86-021-62885108 +8613917661608
info@spring-chem.com China 2068 57
Shanghai Daken Advanced Materials Co.,Ltd
+86-2158073036
info@dakenam.com China 14014 58
ATK CHEMICAL COMPANY LIMITED
+undefined-21-51877795
ivan@atkchemical.com China 33024 60
AB PharmaTech,LLC
323-480-4688
sales@acrospharmatech.com United States 989 55
Beijing Green Guardee Technology Co., Ltd
86-010-69706062
sales2@greenguardee.com CHINA 650 58
career henan chemical co
+86-0371-86658258 +8613203830695
sales@coreychem.com China 29815 58
Xiamen AmoyChem Co., Ltd
+86-86-5926051114 +8615060885618
sales@amoychem.com China 6366 58
BAYNOE CHEM CO.,LTD
+86-21-34783353 +8615000719740
baynoe@baynoe.com CHINA 934 58

602-55-1(9-Phenylanthracen)Verwandte Suche:


  • anthracene,9-phenyl-
  • 9-PHENYLANTHRACENE
  • Phenylanthracene,98%
  • 9-PHENYLANTHRACENE OEKANAL, 250 MG
  • 9-Phenylanthracene97%
  • 9-Phenylanthracene 97%
  • 9-Phenylanthracene,98%
  • NSC 90796
  • 9-phenylantracene
  • 9-PHENYLANTHRACENE OEKANAL
  • 9-Phenylanthracene@50 μg/mL in Toluene
  • 9-Phenylanthracene>
  • 9-phenylanthracene-D9
  • 602-55-1
  • C6H5C14H9
  • C20H14
  • Anthracenes
  • Organic Building Blocks
  • Building Blocks
  • Arenes
  • Building Blocks
  • Chemical Synthesis
  • Organic Building Blocks
  • Aromatics Compounds
  • Anthracenes
  • Aromatics
  • Alpha Sort
  • Chemical Class
  • Hydrocarbons
  • NeatsVolatiles/ Semivolatiles
  • P
  • PAHsAlphabetic
  • PER - POLA
  • P-SAnalytical Standards
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  • Organic Building Blocks
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