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ChemicalBook >> CAS DataBase List >>1,2,3,5-Tetra-O-benzoyl-2-C-methyl-beta-D-ribofuranose

1,2,3,5-Tetra-O-benzoyl-2-C-methyl-beta-D-ribofuranose

CAS No.
15397-15-6
Chemical Name:
1,2,3,5-Tetra-O-benzoyl-2-C-methyl-beta-D-ribofuranose
Synonyms
EOS-60513;(2S,3R,4R,5R)-5-((benzo;1,2,3,5-Tetra-O-benzoyl-2...;b-D-Ribofuranose, 2-C-Methyl-, tetrabenzoate;2-C-Methyl-b-D-ribofuranose 1,2,3,5-tetrabenzoate;2-C-methyl-β-D-Ribofuranose 1,2,3,5-tetrabenzoate;1,2,3,5-Tetra-O-benzoyl-2-C-methyl-β-D-ribofuranose;1,2,3,5-Tetra-O-benzoyl-2-β-C-methyl-D-ribofuranose;2-C-Methyl-beta-D-ribofuranose 1,2,3,5-tetrabenzoate;β-D-Ribofuranose, 2-C-methyl-, 1,2,3,5-tetrabenzoate
CBNumber:
CB21476785
Molecular Formula:
C34H28O9
Molecular Weight:
580.58
MDL Number:
MFCD07369658
MOL File:
15397-15-6.mol
MSDS File:
SDS
Last updated:2026-05-27 23:56:19
Product description Number Pack Size Price
1,2,3,5-Tetra-O-benzoyl-2-C-methyl-Beta-D-ribofuranose TRC-T284220-5G 5g $472
1,2,3,5-Tetra-O-benzoyl-2-C-methyl-Beta-D-ribofuranose TRC-T284220-25MG 25mg $84
1,2,3,5-Tetra-O-benzoyl-2-C-methyl-Beta-D-ribofuranose TRC-T284220-1G 1g $161
1,2,3,5-Tetra-O-benzoyl-2-C-methyl-b-D-ribofuranose MT05623 10g $371.5
1,2,3,5-Tetra-O-benzoyl-2-C-methyl-b-D-ribofuranose MT05623 25g $714.25
More product size

1,2,3,5-Tetra-O-benzoyl-2-C-methyl-beta-D-ribofuranose Properties

Melting point 154-156 °C
Boiling point 687.3±55.0 °C(Predicted)
Density 1.34
storage temp. Sealed in dry,Store in freezer, under -20°C
solubility Soluble in chloroform or acetonitrile
form Powder
color White to Off-white
InChIKey QJZSLTLDMBDKOU-CEPZENHSNA-N
SMILES [C@]1(C)(OC(C2C=CC=CC=2)=O)[C@H](OC(C2=CC=CC=C2)=O)[C@@H](COC(C2=CC=CC=C2)=O)O[C@H]1OC(C1C=CC=CC=1)=O |&1:0,11,21,33,r|

SAFETY

Risk and Safety Statements

Symbol(GHS)  Exclamation Mark (GHS07)
GHS07
Signal word  Warning
Hazard statements  H315-H319-H335
Precautionary statements  P280-P302+P352-P305+P351+P338
HS Code  2932190090

1,2,3,5-Tetra-O-benzoyl-2-C-methyl-beta-D-ribofuranose price More Price(52)

Manufacturer Product number Product description CAS number Packaging Price Updated Buy
TRC TRC-T284220-5G 1,2,3,5-Tetra-O-benzoyl-2-C-methyl-Beta-D-ribofuranose 15397-15-6 5g $472 2026-06-03 Buy
TRC TRC-T284220-25MG 1,2,3,5-Tetra-O-benzoyl-2-C-methyl-Beta-D-ribofuranose 15397-15-6 25mg $84 2026-06-03 Buy
TRC TRC-T284220-1G 1,2,3,5-Tetra-O-benzoyl-2-C-methyl-Beta-D-ribofuranose 15397-15-6 1g $161 2026-06-03 Buy
Biosynth MT05623 1,2,3,5-Tetra-O-benzoyl-2-C-methyl-b-D-ribofuranose 15397-15-6 10g $371.5 2026-06-04 Buy
Biosynth MT05623 1,2,3,5-Tetra-O-benzoyl-2-C-methyl-b-D-ribofuranose 15397-15-6 25g $714.25 2026-06-04 Buy
Product number Packaging Price Buy
TRC-T284220-5G 5g $472 Buy
TRC-T284220-25MG 25mg $84 Buy
TRC-T284220-1G 1g $161 Buy
MT05623 10g $371.5 Buy
MT05623 25g $714.25 Buy

1,2,3,5-Tetra-O-benzoyl-2-C-methyl-beta-D-ribofuranose Chemical Properties,Uses,Production

Chemical Properties

White Powder

Uses

1,2,3,5-Tetra-O-benzoyl-2-C-methyl-β-D-ribofuranose (cas# 15397-15-6) is a compound useful in organic synthesis.

Synthesis

D-Ribonic acid, 2-C-methyl-, γ-lactone, 3,5-dibenzoate

729596-46-7

Benzoyl chloride

98-88-4

1,2,3,5-Tetra-O-benzoyl-2-C-methyl-beta-D-ribofuranose

15397-15-6

1. 100 g (0.27 mol) of 3,5-di-O-benzoyl-2-C-methyl-D-ribofuranose was added to 300 mL of acetonitrile and stirred until completely dissolved. Subsequently 280 mL (2 mol) triethylamine was added. 2. 78.3 mL (0.67 mol) benzoyl chloride was added slowly dropwise at room temperature with controlled titration rate to avoid intense exotherm. 3. After the dropwise addition was completed, the reaction mixture was heated to 60 °C and maintained for 2 hours, during which time the progress of the reaction was monitored by HPLC. 4. Upon completion of the reaction, the mixture was cooled to room temperature and the reaction was quenched by the addition of 150 mL of water. 5. The solid product was collected by filtration, washed with a mixture of acetonitrile/water (2:1, v/v), and subsequently dried under vacuum to constant weight to afford 109 g of 1,2,3,5-tetra-O-benzoyl-2-C-methyl-β-D-ribofuranose in 70% yield. 6. 8.25 kg (22.2 mol) 3,5-di-O-benzoyl-2-C-methyl-D-ribofuranose was dissolved in 21 kg of acetonitrile in a 100 L reactor. 7. 16.8 kg (166.5 mol) of triethylamine was added, followed by the slow dropwise addition of 9.8 kg (69.7 mol) of benzoyl chloride, taking care to control the reaction temperature. 8. The reaction mixture was heated to 60 °C and held for 4 h. 9. 9. After completion of the reaction, the mixture was cooled to room temperature and 13.7 L of water was added slowly and dropwise. 10. The mixture was further cooled to 0 °C and stirred continuously for 1 hour. 11. The solid product was separated by filtration and washed sequentially with 8 L of acetonitrile/water (2:1, v/v) mixture cooled to 0 °C and 4.7 kg of cold methanol.

References

[1] Patent: US2004/158059, 2004, A1. Location in patent: Page 7; 9

30361-17-2
98-88-4
15397-15-6
Synthesis of 1,2,3,5-Tetra-O-benzoyl-2-C-methyl-beta-D-ribofuranose from 2,3,5-Tri-O-benzoyl-2-C-methyl-D-ribofuranose and Benzoyl chloride
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View Lastest Price from 1,2,3,5-Tetra-O-benzoyl-2-C-methyl-beta-D-ribofuranose manufacturers

Image Update time Product Price Min. Order Purity Supply Ability Manufacturer
1,2,3,5-Tetra-O-benzoyl-2-C-methyl-beta-D-ribofuranose pictures 2026-07-22 1,2,3,5-Tetra-O-benzoyl-2-C-methyl-beta-D-ribofuranose
15397-15-6
 1KG 98.0% 500kg/month WUHAN FORTUNA CHEMICAL CO., LTD
1,2,3,5-Tetra-O-benzoyl-2-C-methyl-beta-D-ribofuranose pictures 2021-07-02 1,2,3,5-Tetra-O-benzoyl-2-C-methyl-beta-D-ribofuranose
15397-15-6
 $10.00-15.00 1KG 99%+ HPLC Zhuozhou Wenxi import and Export Co., Ltd
1,2,3,5-Tetra-O-benzoyl-2-C-methyl-beta-D-ribofuranose pictures 2019-07-06 1,2,3,5-Tetra-O-benzoyl-2-C-methyl-beta-D-ribofuranose
15397-15-6
 $1.00 1KG 98% 1tons Career Henan Chemical Co

1,2,3,5-Tetra-O-benzoyl-2-C-methyl-beta-D-ribofuranose Spectrum

2-C-Methyl-beta-D-ribofuranose 1,2,3,5-tetrabenzoate 2-C-Methyl-b-D-ribofuranose 1,2,3,5-tetrabenzoate 1,2,3,5-Tetra-O-benzoyl-2... b-D-Ribofuranose, 2-C-Methyl-, tetrabenzoate 2-C-Methyl-1,2,3,5-tetra-O-benzoyl-beta-D-ribofuranose (2S,3R,4R,5R)-2,4-bis(benzoyloxy)-5-[(benzoyloxy)methyl]-3-methyloxolan-3-yl benzoate 1,2,3,5-tera-o-benzoyl-2'-c-methyl-beta-d-ribofuranose (2S,3R,4R,5R)-5-((benzoyloxy)Methyl)-3-Methyltetrahydrofuran-2,3,4-triyl tribenzoate 1,2,3,5-tetra-O-benzoyl-2-C-methyl-b-D-ribofuranoside 1,2,3,5-Tetra-O-benzoyl-2-C-methyl-beta-D-ribofuranose [(2R,3R,4R,5S)-3,4,5-tribenzoyloxy-4-methyloxolan-2-yl]methyl benzoate TIANFU CHEM 1,2,3,5-Tetra-O-benzoyl-2-C-methyl-beta-D-ribofuranose 1,2,3,5-Tetra-O-benzoyl-2-C-methyl-beta-D-ribofuranose USP/EP/BP 1,2,3,5-Tetra-O-benzoyl-2-C-methyl-β-D-ribofuranose 2-C-Methyl-1,2,3,5-tetra-O-benzoyl-beta-D-ribofuranose 98% "3 4-BIS(BENZOYLOXY)-5-[(BENZOYLOXY)METHYL]-3-METHYLOXOLAN-2-YL BENZOATE (2S,3R,4R,5R)-5-((benzo EOS-60513 1,2,3,5- Tetrabenzoyl -2-C- methyl -beta-D- ribofuranose β-D-Ribofuranose, 2-C-methyl-, 1,2,3,5-tetrabenzoate 2-C-methyl-β-D-Ribofuranose 1,2,3,5-tetrabenzoate 2-?C-?methyl-?,1,?2,?3,?5-?tetrabenzoate-β-?D-?Ribofuranose 1,2,3,5-Tetrakis-O-benzoyl-2-C-methyl-β-D-ribofuranose 1,2,3,5-tetrabenzoyloxy-2-C-Methyl-beta-D-ribofuranose 1,2,3,5-Tetra-O-benzoyl-2-β-C-methyl-D-ribofuranose 15397-15-6 Carbohydrates & Derivatives
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