6-Benzothiazolecarbonitrile,2,3-dihydro-2-thioxo-(9CI)
- CAS No.
- 315228-79-6
- Chemical Name:
- 6-Benzothiazolecarbonitrile,2,3-dihydro-2-thioxo-(9CI)
- Synonyms
- 2-Mercaptobenzothiazole-6-carbonitrile;2-Mercaptobenzo[d]thiazole-6-carbonitrile;2-Mercapto-1,3-benzothiazole-6-carbonitrile;2,3-Dihydro-2-thioxo-6-benzothiazolecarbonitrile;6-Benzothiazolecarbonitrile, 2,3-dihydro-2-thioxo-;2-sulfanylidene-3H-1,3-benzothiazole-6-carbonitrile;6-Benzothiazolecarbonitrile,2,3-dihydro-2-thioxo-(9CI)
- CBNumber:
- CB31272993
- Molecular Formula:
- C8H4N2S2
- Molecular Weight:
- 192.26
- MDL Number:
- MFCD11845316
- MOL File:
- 315228-79-6.mol
- MSDS File:
- SDS
| Product description | Number | Pack Size | Price |
| 2-Mercaptobenzo[d]thiazole-6-carbonitrile 96% | AA00CIXK | 100mg | $7 |
| 2-Mercaptobenzo[d]thiazole-6-carbonitrile 96% | AA00CIXK | 250mg | $16 |
| 2-Mercaptobenzo[d]thiazole-6-carbonitrile 96% | AA00CIXK | 1g | $39 |
| 2-Mercaptobenzo[d]thiazole-6-carbonitrile 96% | AA00CIXK | 5g | $182 |
| 2-Mercaptobenzo[d]thiazole-6-carbonitrile 96% | AA00CIXK | 10g | $363 |
| More product size | |||
6-Benzothiazolecarbonitrile,2,3-dihydro-2-thioxo-(9CI) price
| Manufacturer | Product number | Product description | CAS number | Packaging | Price | Updated | Buy |
|---|---|---|---|---|---|---|---|
| aablocks | AA00CIXK | 2-Mercaptobenzo[d]thiazole-6-carbonitrile 96% | 315228-79-6 | 100mg | $7 | 2026-05-28 | Buy |
| aablocks | AA00CIXK | 2-Mercaptobenzo[d]thiazole-6-carbonitrile 96% | 315228-79-6 | 250mg | $16 | 2026-05-28 | Buy |
| aablocks | AA00CIXK | 2-Mercaptobenzo[d]thiazole-6-carbonitrile 96% | 315228-79-6 | 1g | $39 | 2026-05-28 | Buy |
| aablocks | AA00CIXK | 2-Mercaptobenzo[d]thiazole-6-carbonitrile 96% | 315228-79-6 | 5g | $182 | 2026-05-28 | Buy |
| aablocks | AA00CIXK | 2-Mercaptobenzo[d]thiazole-6-carbonitrile 96% | 315228-79-6 | 10g | $363 | 2026-05-28 | Buy |
6-Benzothiazolecarbonitrile,2,3-dihydro-2-thioxo-(9CI) Chemical Properties,Uses,Production
Synthesis
140-89-6
33348-34-4
315228-79-6
The general procedure for the synthesis of 2-mercaptobenzothiazole-6-carbonitrile from potassium ethylxanthate and 4-amino-3-iodobenzonitrile was as follows: 4-amino-3-iodobenzonitrile (0.6 mmol), potassium ethylxanthate (1.8 mmol), FeF3 (0.06 mmol), 2,2'-bis(diphenylphosphino)-1,1'-binaphthyl ( 0.03 mmol) and DMF (4 mL). The reaction vessel was replaced three times with argon and sealed. Subsequently, the mixture was placed in an oil bath at 110 °C and the reaction was electromagnetically stirred for 3-21 hours. The reaction process was monitored by silica gel thin layer chromatography (TLC). After completion of the reaction, the reaction mixture was cooled to room temperature, 4 mL of 3 mol/L hydrochloric acid solution was added and stirred for 30 min. The reaction mixture was extracted with ethyl acetate (3 x 20 mL). The organic phases were combined, dried with anhydrous sodium sulfate, and finally purified by silica gel column chromatography (eluent: petroleum ether/ethyl acetate) to obtain the target product 2-mercaptobenzothiazole-6-carbonitrile.
References
[1] Synthetic Communications, 2015, vol. 45, # 20, p. 2378 - 2385
[2] Phosphorus, Sulfur and Silicon and the Related Elements, 2016, vol. 191, # 5, p. 699 - 701
6-Benzothiazolecarbonitrile,2,3-dihydro-2-thioxo-(9CI) Preparation Products And Raw materials
| Supplier | Tel | Country | ProdList | Advantage | |
|---|---|---|---|---|---|
| Capot Chemical Co.,Ltd. | +8613336195806 | sales@capot.com | China | 29640 | 60 |
| ATK CHEMICAL COMPANY LIMITED | +undefined-21-51877795 | ivan@atkchemical.com | China | 33024 | 60 |
| CONIER CHEM AND PHARMA LIMITED | +8618523575427 | sales@conier.com | China | 49979 | 58 |
| Career Henan Chemica Co | +86-0371-86658258 +8613203830695 | laboratory@coreychem.com | China | 30225 | 58 |
| HANGZHOU LEAP CHEM CO., LTD. | +86-571-87711850 | market18@leapchem.com | China | 24597 | 58 |
| Jilin Chinese Academy of Sciences-yanshen Technology | +undefined18143011203 | info@chemextension.com | China | 42056 | 58 |
| Aladdin Scientific | tp@aladdinsci.com | United States | 52923 | 58 | |
| Amadis Chemical Company Limited | 571-89925085 | sales@amadischem.com | China | 131957 | 58 |
| JinYan Chemicals(ShangHai) Co.,Ltd. | 13817811078 | sales@jingyan-chemical.com | China | 9976 | 60 |
| Jinan Trio PharmaTech Co., Ltd. | 0531-88811783 | sales@trio-pharmatech.com | China | 1856 | 62 |
