3-Methoxy-2-nitroaniline
- CAS No.
- 16554-47-5
- Chemical Name:
- 3-Methoxy-2-nitroaniline
- Synonyms
- 2-Nitro-3-methoxyaniline;3-Methoxy-2-nitro-phenylamin;3-Methoxy-2-nitro-phenylamine;Benzenamine, 3-methoxy-2-nitro-
- CBNumber:
- CB32620001
- Molecular Formula:
- C7H8N2O3
- Molecular Weight:
- 168.15
- MDL Number:
- MFCD18324417
- MOL File:
- 16554-47-5.mol
- MSDS File:
- SDS
| Product description | Number | Pack Size | Price |
| 3-Methoxy-2-nitroaniline Asreported | 283215 | 50mg | $345 |
| 3-Methoxy-2-nitroaniline Asreported | 283215 | 100mg | $496 |
| 3-Methoxy-2-nitroaniline Asreported | 283215 | 250mg | $761 |
| 3-Methoxy-2-nitroaniline Asreported | 283215 | 500mg | $1055 |
| 3-Methoxy-2-nitroaniline Asreported | 283215 | 1g | $1274 |
| More product size | |||
| Melting point | 124-124.5 °C(Solv: benzene (71-43-2); ligroine (8032-32-4)) |
|---|---|
| Boiling point | 343.6±22.0 °C(Predicted) |
| Density | 1.318±0.06 g/cm3(Predicted) |
| storage temp. | under inert gas (nitrogen or Argon) at 2–8 °C |
| pka | -0.65±0.10(Predicted) |
| form | crystalline powder |
| color | Orange/red and darker crystals |
SAFETY
Risk and Safety Statements
| Symbol(GHS) |  GHS07 |
|---|---|
| Signal word | Warning |
| Hazard statements | H302+H312+H332-H315-H319-H335 |
| Precautionary statements | P271-P260-P280 |
| HS Code | 2921420090 |
3-Methoxy-2-nitroaniline price More Price(54)
| Manufacturer | Product number | Product description | CAS number | Packaging | Price | Updated | Buy |
|---|---|---|---|---|---|---|---|
| Usbiological | 283215 | 3-Methoxy-2-nitroaniline Asreported | 16554-47-5 | 50mg | $345 | 2026-06-03 | Buy |
| Usbiological | 283215 | 3-Methoxy-2-nitroaniline Asreported | 16554-47-5 | 100mg | $496 | 2026-06-03 | Buy |
| Usbiological | 283215 | 3-Methoxy-2-nitroaniline Asreported | 16554-47-5 | 250mg | $761 | 2026-06-03 | Buy |
| Usbiological | 283215 | 3-Methoxy-2-nitroaniline Asreported | 16554-47-5 | 500mg | $1055 | 2026-06-03 | Buy |
| Usbiological | 283215 | 3-Methoxy-2-nitroaniline Asreported | 16554-47-5 | 1g | $1274 | 2026-06-03 | Buy |
3-Methoxy-2-nitroaniline Chemical Properties,Uses,Production
Synthesis
158461-29-1
16554-47-5
General procedure for the synthesis of 2-nitro-3-methoxyaniline from tert-butyl (3-methoxy-2-nitrophenyl)carbamate: to a stirred solution of tert-butyl (3-methoxy-2-nitrophenyl)carbamate (13.3 g, 49.6 mmol) in dichloromethane (100 mL) was added trifluoroacetic acid (20 mL) and the reaction mixture was stirred for 4 hours at room temperature . Subsequently, the mixture was concentrated under vacuum to give a residue which was dissolved in ethyl acetate. The resulting solution was poured into saturated aqueous sodium bicarbonate solution, the organic layer was separated, washed with brine, dried with anhydrous sodium sulfate and concentrated under vacuum. The resulting precipitate was ground with hexane and filtered to afford 2-nitro-3-methoxyaniline (7.55 g, 44.9 mmol, 91% yield) as a yellow solid.1H NMR (CDCl3, 400 MHz): δ 3.88 (3H, s), 6.31 (1H, dd, J = 8.6,1.2 Hz), 7.36 (1H, dd, J = 8.6,1.2Hz), 7.16 (1H, t, J = 8.6Hz).
References
[1] ChemMedChem, 2018, vol. 13, # 19, p. 2090 - 2103
[2] Chemical and Pharmaceutical Bulletin, 1993, vol. 41, # 9, p. 1573 - 1582
[3] Bioorganic and Medicinal Chemistry, 2012, vol. 20, # 5, p. 1644 - 1658
[4] Patent: EP2168959, 2010, A1. Location in patent: Page/Page column 121
[5] Patent: EP2168960, 2010, A1. Location in patent: Page/Page column 61
3-Methoxy-2-nitroaniline Preparation Products And Raw materials
Raw materials
1of2
Preparation Products
| Supplier | Tel | Country | ProdList | Advantage | |
|---|---|---|---|---|---|
| ATK CHEMICAL COMPANY LIMITED | +undefined-21-51877795 | ivan@atkchemical.com | China | 32998 | 60 |
| Accela ChemBio Inc. | +1-858-6993322 +86-18019713315 | info@accelachem.com | United States | 21189 | 58 |
| Alchem Pharmtech,Inc. | 8485655694 | sales@alchempharmtech.com | United States | 63645 | 58 |
| career henan chemical co | +86-0371-86658258 | factory@coreychem.com | China | 29780 | 58 |
| Hefei TNJ Chemical Industry Co.,Ltd. | +86-0551-65418671 +86-189 4982 3763 | sales@tnjchem.com | China | 34526 | 58 |
| Coresyn Pharmatech Co., Ltd. | +86-571-86626709 +86-18157142896 | cbc@coresyn.com | China | 9976 | 58 |
| Aromsyn Co., Ltd. | +86-0571-85585865 +86-13336024896 | CB@aromsyn.com | China | 19176 | 58 |
| Aceschem Inc. | +1-817863-6948 +1-（817）863-6948 | sales@aceschem.com | United States | 19621 | 58 |
| Nanjing Fred Technology Co., Ltd | +86-25-84696168 +86-15380713688 | Austin@fredbio.com | China | 2428 | 58 |
| Nanjing Bicbiotechnology Co., Ltd | +86-2552131256 +86-18251840740 | sales@bicbiotech.com | China | 5990 | 58 |
View Lastest Price from 3-Methoxy-2-nitroaniline manufacturers
| Image | Update time | Product | Price | Min. Order | Purity | Supply Ability | Manufacturer | |
|---|---|---|---|---|---|---|---|---|
 |
2020-02-02 | 3-Methoxy-2-nitroaniline
16554-47-5
|
$1.00 | 1KG | 97% | 100kg | Career Henan Chemical Co |
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- 3-Methoxy-2-nitroaniline
16554-47-5
- $1.00
- 97%
- Career Henan Chemical Co
