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ChemicalBook >> CAS DataBase List >>2-Bromo-9,9-dihexyl fluorene

2-Bromo-9,9-dihexyl fluorene

CAS No.
226070-05-9
Chemical Name:
2-Bromo-9,9-dihexyl fluorene
Synonyms
2-Bromo-9,9-dihexyl-9H-fluorene;2-Bromo-9,9-di-n-hexylfluoren;9,9-Dihexyl-2-bromofluorene;2-Bromo-9,9-dihexyl fluorene;2-Bromo-9,9-dihexylfluorene>9H-Fluorene, 2-broMo-9,9-dihexyl-;2-Bromo-9,9-dihexyl fluorene ISO 9001:2015 REACH
CBNumber:
CB42535850
Molecular Formula:
C25H33Br
Molecular Weight:
413.43
MDL Number:
MFCD14584649
MOL File:
226070-05-9.mol
MSDS File:
SDS
Last updated:2026-05-28 02:31:36
Product description Number Pack Size Price
2-Bromo-9,9-dihexylfluorene >97.0%(GC) B4404 1g $124
2-Bromo-9,9-dihexylfluorene >97.0%(GC) B4404 200mg $43
2-Bromo-9,9-dihexyl-9H-fluorene 97% AA00BBVN 1g $8
2-Bromo-9,9-dihexyl-9H-fluorene 97% AA00BBVN 5g $29
2-Bromo-9,9-dihexyl-9H-fluorene 97% AA00BBVN 25g $54
More product size

2-Bromo-9,9-dihexyl fluorene Properties

Boiling point 485.3±24.0 °C(Predicted)
Density 1.116±0.06 g/cm3(Predicted)
refractive index 1.5680-1.5720
storage temp. Sealed in dry,Room Temperature
form clear liquid to slightly cloudy liquid
color Light yellow to Brown
λmax 309nm(THF)(lit.)

SAFETY

Risk and Safety Statements

Symbol(GHS)  Exclamation Mark (GHS07)
GHS07
Signal word  Warning
Hazard statements  H315-H319
Precautionary statements  P264-P280-P302+P352+P332+P313+P362+P364-P305+P351+P338+P337+P313
HS Code  2903.99.8001

2-Bromo-9,9-dihexyl fluorene price More Price(20)

Manufacturer Product number Product description CAS number Packaging Price Updated Buy
TCI Chemical B4404 2-Bromo-9,9-dihexylfluorene >97.0%(GC) 226070-05-9 1g $124 2026-04-30 Buy
TCI Chemical B4404 2-Bromo-9,9-dihexylfluorene >97.0%(GC) 226070-05-9 200mg $43 2026-04-30 Buy
aablocks AA00BBVN 2-Bromo-9,9-dihexyl-9H-fluorene 97% 226070-05-9 1g $8 2026-05-28 Buy
aablocks AA00BBVN 2-Bromo-9,9-dihexyl-9H-fluorene 97% 226070-05-9 5g $29 2026-05-28 Buy
aablocks AA00BBVN 2-Bromo-9,9-dihexyl-9H-fluorene 97% 226070-05-9 25g $54 2026-05-28 Buy
Product number Packaging Price Buy
B4404 1g $124 Buy
B4404 200mg $43 Buy
AA00BBVN 1g $8 Buy
AA00BBVN 5g $29 Buy
AA00BBVN 25g $54 Buy

2-Bromo-9,9-dihexyl fluorene Chemical Properties,Uses,Production

Synthesis

1-Bromohexane

111-25-1

2-Bromofluorene

1133-80-8

2-Bromo-9,9-dihexyl fluorene

226070-05-9

Example 1: Synthesis of 2-bromo-9,9-dihexylfluorene 1. 2-Bromofluorene (9.8 g, 1.0 equiv), 1-bromohexane (39.6 g, excess), tetrabutylammonium bromide (2.58 g, phase transfer catalyst), and 50% aqueous NaOH (75 mL) were sequentially added to a 250 mL round-bottom flask. 2. The reaction mixture was stirred at 80 °C overnight (about 12 hours). 3. After completion of the reaction, the reaction was cooled to room temperature and the organic layer was separated. 4. 4. The aqueous phase was extracted with ether (3 x 50 mL) and the organic phases were combined. 5. The organic phase was washed with saturated saline (100 mL) and dried over anhydrous magnesium sulfate. 6. The solvent was evaporated under pressure reduction, and the crude product was purified by short silica gel column chromatography to obtain 15.45 g of white solid product in 93.8% yield. Precautions. - 1-Bromohexane needs to be greatly overdosed to ensure complete reaction. - Tetrabutylammonium bromide as phase transfer catalyst can significantly improve the reaction efficiency. - The reaction temperature should be strictly controlled at 80 °C to avoid side reactions. - Petroleum ether/ethyl acetate (20:1) can be used as eluent for silica gel column chromatography.

References

[1] Journal of the American Chemical Society, 2005, vol. 127, # 33, p. 11763 - 11768
[2] Organometallics, 2013, vol. 32, # 2, p. 460 - 467
[3] Tetrahedron Letters, 2007, vol. 48, # 6, p. 919 - 923
[4] Journal of Organic Chemistry, 2010, vol. 75, # 8, p. 2714 - 2717
[5] Chemical Communications, 2002, # 7, p. 784 - 785

2-Bromo-9,9-dihexyl fluorene Preparation Products And Raw materials

Global( 87)Suppliers
Supplier Tel Email Country ProdList Advantage
Henan Fengda Chemical Co., Ltd
+86-371-86557731 +86-13613820652 info@fdachem.com China 20120 58
Shanghai Daken Advanced Materials Co.,Ltd
+86-2158073036 info@dakenam.com China 14026 58
ATK CHEMICAL COMPANY LIMITED
+undefined-21-51877795 ivan@atkchemical.com China 33024 60
AB PharmaTech,LLC
323-480-4688 sales@acrospharmatech.com United States 989 55
career henan chemical co
+86-0371-86658258 sales@coreychem.com China 29812 58
Fuxin Pharmaceutical
+86-021-021-50872116 contact@fuxinpharm.com China 9976 58
Antai Fine Chemical Technology Co.,Limited
18503026267 info@antaichem.com CHINA 9636 58
SHANGHAI T&W PHARMACEUTICAL CO., LTD.
+86-021-61551413 contact@trustwe.com China 5746 58
Zhengzhou Alfa Chemical Co.,Ltd
+86-18530059196 sale04@alfachem.cn China 9612 58
ANHUI WITOP BIOTECH CO., LTD
+8618071025641 eric@witopchemical.com China 23541 58

View Lastest Price from 2-Bromo-9,9-dihexyl fluorene manufacturers

Image Update time Product Price Min. Order Purity Supply Ability Manufacturer
2-Bromo-9,9-dihexylfluorene pictures 2026-07-09 2-Bromo-9,9-dihexylfluorene
226070-05-9
$1.00-200.00 1KG 99%, 99.5% Sublimated Henan Fengda Chemical Co., Ltd
2-Bromo-9,9-dihexyl fluorene pictures 2026-07-09 2-Bromo-9,9-dihexyl fluorene
226070-05-9
$1.00-188.00 1KG 99%, 99.5% Sublimated Henan Fengda Chemical Co., Ltd
2-Bromo-9,9-di-n-hexylfluoren pictures 2025-07-02 2-Bromo-9,9-di-n-hexylfluoren
226070-05-9
1KG 98% 150KG /month Shanghai Daken Advanced Materials Co.,Ltd

2-Bromo-9,9-dihexyl fluorene Spectrum

2-Bromo-9,9-dihexyl fluorene 9H-Fluorene, 2-broMo-9,9-dihexyl- 2-Bromo-9,9-dihexylfluorene> 2-Bromo-9,9-dihexyl fluorene ISO 9001:2015 REACH 9,9-Dihexyl-2-bromofluorene 2-Bromo-9,9-dihexyl-9H-fluorene 2-Bromo-9,9-di-n-hexylfluoren 226070-05-9 C25H33Br
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