2,6-Dichloro-4-iodophenol
- CAS No.
- 34074-22-1
- Chemical Name:
- 2,6-Dichloro-4-iodophenol
- Synonyms
- 2,6-Dichloro-4-iodophenol;Phenol, 2,6-dichloro-4-iodo-;2,6-Dichloro-4-iodophenol 98%;2,6-dichloro-4-iodobenzenephenol
- CBNumber:
- CB52665365
- Molecular Formula:
- C6H3Cl2IO
- Molecular Weight:
- 288.9
- MDL Number:
- MFCD00466446
- MOL File:
- 34074-22-1.mol
- MSDS File:
- SDS
| Product description | Number | Pack Size | Price |
| 2,6-Dichloro-4-iodophenol >98% | OR321013 | 1g | $21 |
| 2,6-Dichloro-4-iodophenol >98% | OR321013 | 5g | $43 |
| 2,6-Dichloro-4-iodophenol >98% | OR321013 | 25g | $199 |
| 2,6-Dichloro-4-iodophenol >98% | OR321013 | 100g | $691 |
| 2,6-Dichloro-4-iodophenol 98% | AS41766 | 1g | $26 |
| More product size | |||
2,6-Dichloro-4-iodophenol price More Price(26)
| Manufacturer | Product number | Product description | CAS number | Packaging | Price | Updated | Buy |
|---|---|---|---|---|---|---|---|
| Apolloscientific | OR321013 | 2,6-Dichloro-4-iodophenol >98% | 34074-22-1 | 1g | $21 | 2026-06-04 | Buy |
| Apolloscientific | OR321013 | 2,6-Dichloro-4-iodophenol >98% | 34074-22-1 | 5g | $43 | 2026-06-04 | Buy |
| Apolloscientific | OR321013 | 2,6-Dichloro-4-iodophenol >98% | 34074-22-1 | 25g | $199 | 2026-06-04 | Buy |
| Apolloscientific | OR321013 | 2,6-Dichloro-4-iodophenol >98% | 34074-22-1 | 100g | $691 | 2026-06-04 | Buy |
| Activate Scientific | AS41766 | 2,6-Dichloro-4-iodophenol 98% | 34074-22-1 | 1g | $26 | 2026-06-04 | Buy |
2,6-Dichloro-4-iodophenol Chemical Properties,Uses,Production
Synthesis
87-65-0
34074-22-1
The general procedure for the synthesis of 2,6-dichloro-4-iodophenol from 2,6-dichlorophenol was as follows: 2,6-dichlorophenol (10 g, 61.35 mmol, 1.00 eq.) and N-iodosuccinimide (NIS, 27.6 g, 245.33 mmol, 2.00 eq.) were dissolved in methanol (100 mL) and stirred at room temperature for 1 hour. After completion of the reaction, the mixture was concentrated under reduced pressure. The concentrated residue was redissolved in ethyl acetate (50 mL) and washed with saturated saline (3 x 30 mL). The organic layer was dried over anhydrous sodium sulfate and concentrated under reduced pressure. The residue was purified by silica gel column chromatography using petroleum ether (100%) as eluent to afford 2,6-dichloro-4-iodophenol (10.5 g, 59% yield) as a yellow solid.1H-NMR (300 MHz, CDCl3): δ 9.83 (s, 1H), 7.27 (s, 2H) ppm.
References
[1] Patent: WO2006/100026, 2006, A1. Location in patent: Page/Page column 121
[2] Synthetic Communications, 2014, vol. 44, # 14, p. 2094 - 2102
[3] Journal of the Brazilian Chemical Society, 2010, vol. 21, # 4, p. 770 - 774
[4] Synthetic Communications, 2012, vol. 42, # 16, p. 2407 - 2414
[5] Advanced Synthesis and Catalysis, 2013, vol. 355, # 14-15, p. 2936 - 2941
2,6-Dichloro-4-iodophenol Preparation Products And Raw materials
| Supplier | Tel | Country | ProdList | Advantage | |
|---|---|---|---|---|---|
| Shanghai Daken Advanced Materials Co.,Ltd | +86-2158073036 | info@dakenam.com | China | 14032 | 58 |
| Speranza Chemical Co., Ltd. | +86-86-075521030354 +86-18688942810 | sophieliu@speranzachem.com | China | 923 | 55 |
| Alchem Pharmtech,Inc. | 8485655694 | sales@alchempharmtech.com | United States | 63645 | 58 |
| Zhengzhou Alfa Chemical Co.,Ltd | +86-18530059196 | sale04@alfachem.cn | China | 9609 | 58 |
| Hefei TNJ Chemical Industry Co.,Ltd. | +86-0551-65418671 +86-189 4982 3763 | sales@tnjchem.com | China | 34526 | 58 |
| Win-Win chemical CO., Limited | +86-0086-577-64498589 +86-15355981851 | sales@win-winchemical.com | China | 14301 | 58 |
| Labnetwork lnc. | +86-27-50766799 +86-18062016861 | contact@labnetwork.com | China | 19981 | 58 |
| HANGZHOU LEAP CHEM CO., LTD. | +86-571-87711850 +8619957148339 | market18@leapchem.com | China | 24569 | 58 |
| Aromsyn Co., Ltd. | +86-0571-85585865 +86-13336024896 | CB@aromsyn.com | China | 19176 | 58 |
| Hebei Chuanghai Biotechnology Co., Ltd | +86-17732866630 | mina@chuanghaibio.com | China | 18114 | 58 |
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