2-NITRO-3-ACETYLAMINO-4-METHYLBENZOIC ACID
- CAS No.
- 7356-52-7
- Chemical Name:
- 2-NITRO-3-ACETYLAMINO-4-METHYLBENZOIC ACID
- Synonyms
- 3-Acetamido-4-methyl-2-nitrobenzoic acid;2-NITRO-3-ACETYLAMINO-4-METHYLBENZOIC ACID;3-Acetylamino-4-methyl-2-nitro-benzoic acid;Benzoic acid, 3-(acetylaMino)-4-Methyl-2-nitro-
- CBNumber:
- CB6310714
- Molecular Formula:
- C10H10N2O5
- Molecular Weight:
- 238.2
- MDL Number:
- MFCD00755098
- MOL File:
- 7356-52-7.mol
- MSDS File:
- SDS
| Product description | Number | Pack Size | Price |
| 3-Acetamido-4-methyl-2-nitrobenzoic acid 98%(HPLC) | W8164 | 250mg | $16 |
| 3-Acetamido-4-methyl-2-nitrobenzoic acid 98%(HPLC) | W8164 | 1g | $39 |
| 3-Acetamido-4-methyl-2-nitrobenzoic acid 98%(HPLC) | W8164 | 5g | $114 |
| 3-Acetamido-4-methyl-2-nitrobenzoic acid 98%(HPLC) | W8164 | 10g | $194 |
| 3-Acetamido-4-methyl-2-nitrobenzoic acid 98%(HPLC) | W8164 | 25g | $398 |
2-NITRO-3-ACETYLAMINO-4-METHYLBENZOIC ACID price More Price(67)
| Manufacturer | Product number | Product description | CAS number | Packaging | Price | Updated | Buy |
|---|---|---|---|---|---|---|---|
| AK Scientific | W8164 | 3-Acetamido-4-methyl-2-nitrobenzoic acid 98%(HPLC) | 7356-52-7 | 250mg | $16 | 2026-06-04 | Buy |
| AK Scientific | W8164 | 3-Acetamido-4-methyl-2-nitrobenzoic acid 98%(HPLC) | 7356-52-7 | 1g | $39 | 2026-06-04 | Buy |
| AK Scientific | W8164 | 3-Acetamido-4-methyl-2-nitrobenzoic acid 98%(HPLC) | 7356-52-7 | 5g | $114 | 2026-06-04 | Buy |
| AK Scientific | W8164 | 3-Acetamido-4-methyl-2-nitrobenzoic acid 98%(HPLC) | 7356-52-7 | 10g | $194 | 2026-06-04 | Buy |
| AK Scientific | W8164 | 3-Acetamido-4-methyl-2-nitrobenzoic acid 98%(HPLC) | 7356-52-7 | 25g | $398 | 2026-06-04 | Buy |
2-NITRO-3-ACETYLAMINO-4-METHYLBENZOIC ACID Chemical Properties,Uses,Production
Synthesis
6946-14-1
7356-52-7
The general procedure for the synthesis of 3-acetamido-4-methyl-2-nitrobenzoic acid from 3-acetamido-4-methylbenzoic acid is as follows: in Example 42, 3-acetamido-4-methylbenzoic acid (205 g, 1061 mmol) was added in batches to stirred fuming nitric acid (1 L), keeping the reaction temperature at -5°C during the addition process and ensuring that the entire reaction temperature does not exceed 0 °C throughout the reaction. After the addition was completed, stirring of the reaction mixture was continued for 1 hour. Subsequently, crushed ice (2.5 kg) was added to the reaction mixture and stirring was continued for 30 minutes. At the end of the reaction, the precipitate formed was collected by filtration and washed thoroughly with water. The obtained filter cake was air-dried and suspended in 1 L of acetic acid at 65°C. The suspension was allowed to stand for 1 hour to naturally cool to room temperature and then filtered. The filtrate was washed with acetic acid and ether sequentially to finally obtain 3-acetamido-4-methyl-2-nitrobenzoic acid (160 g, 63% yield) as a white solid. Mass spectrometry analysis showed (M + H)+ of 239.
References
[1] Patent: WO2018/218070, 2018, A2. Location in patent: Page/Page column 181; 182
[2] Patent: WO2007/76092, 2007, A2. Location in patent: Page/Page column 71
[3] Patent: WO2015/27222, 2015, A2. Location in patent: Paragraph 0278
[4] Patent: WO2007/125405, 2007, A2. Location in patent: Page/Page column 27; 87
[5] Patent: US2004/167194, 2004, A1. Location in patent: Page 23
2-NITRO-3-ACETYLAMINO-4-METHYLBENZOIC ACID Preparation Products And Raw materials
2-NITRO-3-ACETYLAMINO-4-METHYLBENZOIC ACID Suppliers
| Supplier | Tel | Country | ProdList | Advantage | |
|---|---|---|---|---|---|
| Alchem Pharmtech,Inc. | 8485655694 | sales@alchempharmtech.com | United States | 63687 | 58 |
| career henan chemical co | +86-0371-86658258 +8613203830695 | factory@coreychem.com | China | 29792 | 58 |
| sgtlifesciences pvt ltd | +8617013299288 | dj@sgtlifesciences.com | China | 12373 | 58 |
| ShenZhen Trendseen Biological Technology Co.,Ltd. | 13417589054 | trendseenbio@gmail.com | China | 11681 | 58 |
| Aladdin Scientific | tp@aladdinsci.com | United States | 52923 | 58 | |
| DAYANG CHEM (HANGZHOU) CO.,LTD | +86-88938639 +86-17705817739 | info@dycnchem.com | China | 53803 | 58 |
| Amadis Chemical Company Limited | 571-89925085 | sales@amadischem.com | China | 131957 | 58 |
| Shanghai Sunway Pharmaceutical Technology Co., Ltd | 13761987713 | hxzheng@sunwaypharm.cn | China | 8666 | 57 |
| Hangzhou Sage Chemical Co., Ltd. | +86057186818502 13588463833 | info@sagechem.com | China | 10266 | 58 |
| Wuhan TCASChem Technology Co., Ltd. | 027-86697669 13986148687 | sales@tcaschem.com | China | 3986 | 55 |
View Lastest Price from 2-NITRO-3-ACETYLAMINO-4-METHYLBENZOIC ACID manufacturers
| Image | Update time | Product | Price | Min. Order | Purity | Supply Ability | Manufacturer | |
|---|---|---|---|---|---|---|---|---|
 |
2020-01-09 | 2-NITRO-3-ACETYLAMINO-4-METHYLBENZOIC ACID
7356-52-7
|
$6.68 | 1KG | 97%-99% | 1kg-1000kg | Career Henan Chemical Co |
-
- 2-NITRO-3-ACETYLAMINO-4-METHYLBENZOIC ACID
7356-52-7
- $6.68
- 97%-99%
- Career Henan Chemical Co
