1-(2,4,5-trichlorophenyl)ethan-1-one
- CAS No.
- 13061-28-4
- Chemical Name:
- 1-(2,4,5-trichlorophenyl)ethan-1-one
- Synonyms
- Einecs 235-954-9;Ceftizoxime Impurity 34;2',4',5'-Trichloroacetophenone;1-(2,4,5-trichlorophenyl)ethanone;Ethanone,1-(2,4,5-trichlorophenyl)-;1-(2,4,5-trichlorophenyl)ethan-1-one
- CBNumber:
- CB8919492
- Molecular Formula:
- C8H5Cl3O
- Molecular Weight:
- 223.48
- MDL Number:
- MFCD09261422
- MOL File:
- 13061-28-4.mol
- MSDS File:
- SDS
| Product description | Number | Pack Size | Price |
| 2',4',5'-Trichloroacetophenone 95% | OR61087 | 100mg | $21 |
| 2',4',5'-Trichloroacetophenone 95% | OR61087 | 250mg | $28 |
| 2',4',5'-Trichloroacetophenone 95% | OR61087 | 1g | $108 |
| 1-(2,4,5-Trichlorophenyl)ethanone 98% | AS45961 | 1g | $146 |
| 1-(2,4,5-Trichlorophenyl)ethanone 98% | AS45961 | 5g | $446 |
| storage temp. | Sealed in dry,Room Temperature |
|---|---|
| form | fused solid |
| color | White |
| FDA UNII | O9M4U4I96I |
SAFETY
Risk and Safety Statements
| Symbol(GHS) |  GHS07 |
|---|---|
| Signal word | Warning |
| Hazard statements | H302-H315-H319-H332-H335 |
| Precautionary statements | P261-P280-P305+P351+P338 |
| HS Code | 2914790090 |
1-(2,4,5-trichlorophenyl)ethan-1-one price More Price(41)
| Manufacturer | Product number | Product description | CAS number | Packaging | Price | Updated | Buy |
|---|---|---|---|---|---|---|---|
| Apolloscientific | OR61087 | 2',4',5'-Trichloroacetophenone 95% | 13061-28-4 | 100mg | $21 | 2026-06-04 | Buy |
| Apolloscientific | OR61087 | 2',4',5'-Trichloroacetophenone 95% | 13061-28-4 | 250mg | $28 | 2026-06-04 | Buy |
| Apolloscientific | OR61087 | 2',4',5'-Trichloroacetophenone 95% | 13061-28-4 | 1g | $108 | 2026-06-04 | Buy |
| Activate Scientific | AS45961 | 1-(2,4,5-Trichlorophenyl)ethanone 98% | 13061-28-4 | 1g | $146 | 2026-06-04 | Buy |
| Activate Scientific | AS45961 | 1-(2,4,5-Trichlorophenyl)ethanone 98% | 13061-28-4 | 5g | $446 | 2026-06-04 | Buy |
1-(2,4,5-trichlorophenyl)ethan-1-one Chemical Properties,Uses,Production
Synthesis
75-36-5
120-82-1
13061-28-4
Acetyl chloride (11.8 g, 150 mmol) was slowly added dropwise to a stirred mixture of 1,2,4-trichlorobenzene (18.2 g, 100 mmol) and anhydrous aluminum trichloride (33.4 g, 250 mmol) at room temperature. The reaction mixture was then gradually heated to 120-125°C (oil bath heating) and the reaction was maintained at this temperature for 3 hours. Upon completion of the reaction, the resulting viscous mixture was carefully poured into ice water (125 mL) to quench the reaction, followed by extraction of the aqueous phase with dichloromethane (3 x 70 mL). The organic phases were combined, dried with anhydrous magnesium sulfate, filtered and the solvent concentrated under reduced pressure. The residue was purified by distillation under reduced pressure to give a colorless liquid product which solidified to a solid after standing at room temperature. Yield: 15.6 g (82% yield); melting point: 43-45 °C, boiling point: 135 °C/6 mmHg (literature values: melting point 47 °C [29]; 44-46 °C [30]; 45.5-46 °C [31], boiling point 114-116 °C/2 mmHg [31]).
References
[1] Zeitschrift fur Naturforschung - Section B Journal of Chemical Sciences, 2017, vol. 72, # 5, p. 369 - 375
[2] Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1977, p. 1541 - 1544
1-(2,4,5-trichlorophenyl)ethan-1-one Preparation Products And Raw materials
1-(2,4,5-trichlorophenyl)ethan-1-one Suppliers
| Supplier | Tel | Country | ProdList | Advantage | |
|---|---|---|---|---|---|
| SUZHOU SENFEIDA CHEMICAL CO.,LTD | +86-0512-83500002 +86-15195660023 | 3899766280@qq.com | China | 26362 | 58 |
| HANGZHOU LEAP CHEM CO., LTD. | +86-571-87711850 +86-15355479329 | market18@leapchem.com | China | 43333 | 58 |
| Shanghai Acmec Biochemical Technology Co., Ltd. | +86-18621343501 | product@acmec-e.com | China | 33324 | 58 |
| Aladdin Scientific | tp@aladdinsci.com | United States | 52923 | 58 | |
| SHANGHAI KEAN TECHNOLOGY CO., LTD. | +8613817748580 | cooperation@kean-chem.com | China | 40066 | 58 |
| Amadis Chemical Company Limited | 571-89925085 | sales@amadischem.com | China | 131956 | 58 |
| Shanghai Synteam Biochem CO.,ltd | +86-021-58380978 13482386415 | info@systeambc.com | China | 898 | 50 |
| Shanghai Jovan Biochemical Technology Co. Ltd. | +86-021-61654350 | 1245958370@qq.com | China | 2982 | 50 |
| BePharm Ltd | 400-685-9117 | market@bepharm.com | China | 15081 | 60 |
| Nanjing KaiMubo Pharmaceutical Co., Ltd. | 025-66162170 | China | 7181 | 55 |
