ChemicalBook >?? ???? >?? ??>??? ???> tert-Butyl 3,9-diazaspiro[5.5]undecane-3-carboxylate

tert-Butyl 3,9-diazaspiro[5.5]undecane-3-carboxylate

tert-Butyl 3,9-diazaspiro[5.5]undecane-3-carboxylate ??? ???

?? ??:: 173405-78-2

???:: tert-Butyl 3,9-diazaspiro[5.5]undecane-3-carboxylate

???(??):: TERT-BUTYL 3,9-DIAZASPIRO[5.5]UNDECANE-3-CARBOXYLATE;3,9-Diazaspiro[5.5]undecane-3-carboxylic acid, 1,1-dimethylethyl ester;3-Boc-3,9-diazaspiro[5.5]...;3-Boc-3,9-Diazaspiro[5.5]undecane;3-N-Boc-3,9-diazaspiro[5.5]undecane;3-Boc-3,9-diazaspiro[5.5]undecane heMioxalate;Tert-Butyl3,9-Diazaspiro[5.5]Undecane-3-Carboxyla;tert-Butyl 3,9-diazaspiro5.5undecan-3-carboxylate;3,9-Diazaspiro[5,5]undecane-3-carboxylate tert-butyl ester;3,9-DIAZASPIRO[5.5]UNDECANE-3-CARBOXYLIC ACID T-BUTYL ESTER

CBNumber:: CB5434952

???:: C14H26N2O2

??? ??:: 254.37

MOL ??:: 173405-78-2.mol

?? ?? 200

tert-Butyl 3,9-diazaspiro[5.5]undecane-3-carboxylate ??

???: 0°C

?? ?: 0°C

??: 1.05

???: 0°C

?? ??: 2-8°C(protect from light)

??? ??: ??

??? ??: ??? ??

?? ?? (pKa): 11.00±0.20(Predicted)

??: ???

InChI: InChI=1S/C14H26N2O2/c1-13(2,3)18-12(17)16-10-6-14(7-11-16)4-8-15-9-5-14/h15H,4-11H2,1-3H3

InChIKey: YLKHACHFJMCIRE-UHFFFAOYSA-N

SMILES: C1C2(CCNCC2)CCN(C(OC(C)(C)C)=O)C1

?? ? ?? ??
?? ? ???? ?? (GHS)

?? ???? ??	36/37/38-20/21/22-68
?????	26-36-36/37/39-28
HS ??	29339900

????(GHS):

?? ?:

Warning

??·?? ??:

??	??·?? ??	?? ??	??	?? ?	P- ??
H302	??? ???	?? ?? ?? - ??	?? 4	??	P264, P270, P301+P312, P330, P501
H315	??? ??? ???	????? ?? ?????	?? 2	??	P264, P280, P302+P352, P321,P332+P313, P362
H319	?? ?? ??? ???	?? ? ?? ?? ??? ??	?? 2A	??	P264, P280, P305+P351+P338,P337+P313P
H335	?? ???? ??? ? ??	?? ???? ?? - 1? ??;???? ??	?? 3	??

??????:

P261	??·?·??·???·??·...·????? ??? ????.
P280	????/???/???/?????? ?????.
P304+P340	???? ??? ??? ?? ??? ??? ???? ?? ??? ??? ????.
P305+P351+P338	?? ??? ? ?? ?? ???? ????. ???? ?????? ?????. ?? ????.

tert-Butyl 3,9-diazaspiro[5.5]undecane-3-carboxylate C??? ??, ??, ??

Synthesis

Under argon atmosphere, wet Pd/C (188.05 mg, 159.50 μmol, purity 10%) was added into tert-butyl 9-benzyl-3,9-diazaspiro[5.5]undecane-3-carboxylate in THF solution (1.10 g, 3.19 mmol), after replacing the gas in the flask 3 times with hydrogen, the reaction was stirred at 40°C for 40 hours under 45 Psi. After completion of the reaction, the solution was filtered through diatomite. The filtrate was concentrated to give the crude tert-Butyl 3,9-diazaspiro[5.5]undecane-3-carboxylate.

tert-Butyl 3,9-diazaspiro[5.5]undecane-3-carboxylate ?? ?? ? ???

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tert-Butyl 3,9-diazaspiro[5.5]undecane-3-carboxylate ?? ??

???( 200)?? ??

???	??	???	??	?? ?	??
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tert-Butyl 3,9-diazaspiro[5.5]undecane-3-carboxylate ?? ??:

3,6-Diaza-bicyclo[3.1.1]heptane-3-carboxylic acid tert-butyl ester 9-Boc-3,9-diaza-bicyclo[3.3.1]nonane 2-Oxo-1-oxa-3,9-diaza-spiro[5.5]undecane-9-carboxylic acid tert-butyl ester 1,4-DIAZA-SPIRO[5.5]UNDECANE-1-CARBOXYLIC ACID TERT-BUTYL ESTER 1,4-DIAZA-SPIRO[5.5]UNDECANE-4-CARBOXYLIC ACID TERT-BUTYL ESTER 9-BENZYL-3,9-DIAZA-SPIRO[5.5]UNDECANE-3-CARBOXYLIC ACID TERT-BUTYL ESTER 3-METHYL-3,9-DIAZASPIRO[5.5]UNDECANE 4-(2-Aminoethyl)-1-Boc-piperidine (2-PIPERIDIN-4-YL-ETHYL)-CARBAMIC ACID TERT-BUTYL ESTER tert-Butyl 3,9-diazaspiro[5.5]undecane-3-carboxylate

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