ChemicalBook CAS DataBase List 3-methyl-1,2,3,4-tetrahydroquinoline-8-sulfonic acid

3-methyl-1,2,3,4-tetrahydroquinoline-8-sulfonic acid synthesis

2synthesis methods

Product Name:3-methyl-1,2,3,4-tetrahydroquinoline-8-sulfonic acid
CAS Number:153886-68-1
Molecular formula:C10H13NO3S
Molecular Weight:227.28

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3-methyl-1,2,3,4-tetrahydroquinoline-8-sulfonic acid

153886-68-1
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Yield:-

Steps:

Multi-step reaction with 2 steps
1.1: ClSO₃H / 140 °C
1.2: 96 percent / water
2.1: 69 percent / H₂; aq. HCl / Rh-C / 16 h / 70 °C

References:

Altenburger, Jean-Michel;Lassalle, Gilbert Y.;Matrougui, Mostapha;Galtier, Daniel;Jetha, Jean-Claude;Bocskei, Zsolt;Berry, Christopher N.;Lunven, Catherine;Lorrain, Janine;Herault, Jean-Pascal;Schaeffer, Paul;O'Connor, Stephen E.;Herbert, Jean-Marc [Bioorganic and Medicinal Chemistry,2004,vol. 12,# 7,p. 1713 - 1730]

153886-69-2
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153886-68-1
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References

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3-methyl-1,2,3,4-tetrahydroquinoline-8-sulfonic acid synthesis

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