ChemicalBook >?? ???? >?? ???>OLED ?? ???>???,B-[4-(1-??-1H-??????-2-?)??]-

???,B-[4-(1-??-1H-??????-2-?)??]-

???,B-[4-(1-??-1H-??????-2-?)??]- ??? ???

?? ??:: 952514-79-3

???:: ???,B-[4-(1-??-1H-??????-2-?)??]-

???(??):: ???,B-[4-(1-??-1H-??????-2-?)??]-

???:: 4-(1-Phenyl-1H-benzimidazol-2-yl)phenylboronic acid

???(??):: BIBA;(4-(1-Phenyl-1H-benzo[d]imidazol-2-yl);1-Phenyl-2-(4-phenylboronic acid)-benzimidazole;1-phenyl-2-(phenyl-4-boronic acid)-benzimidazole;[4-(1-phenylbenzimidazol-2-yl)phenyl]boronic acid;1-phenyl-2-( phenyl-4-boromic acid)-benzimidazole;4-(1-Phenyl-1H-benzimidazol-2-yl)phenylboronic acid;[1,3,2]dioxaborolan-2-yl)-phenyl]-1H-benzoiMidazole;4-(1-Phenyl-1H-benzimidazol-2-yl)benzeneboronic Acid;[3-(1-phenyl-1H-benziMidazol-2-yl)phenyl]Boronic acid

CBNumber:: CB61512645

???:: C19H15BN2O2

??? ??:: 314.15

MOL ??:: 952514-79-3.mol

?? ?? 157

???,B-[4-(1-??-1H-??????-2-?)??]- ??

?? ?: 572.6±60.0 °C(Predicted)

??: 1.21±0.1 g/cm3(Predicted)

?? ??: under inert gas (nitrogen or Argon) at 2-8°C

???: ???? ???

??? ??: powder to crystal

?? ?? (pKa): 8.47±0.17(Predicted)

??: White to Light yellow to Light orange

InChI: InChI=1S/C19H15BN2O2/c23-20(24)15-12-10-14(11-13-15)19-21-17-8-4-5-9-18(17)22(19)16-6-2-1-3-7-16/h1-13,23-24H

InChIKey: PBSIVXAPTBHFFV-UHFFFAOYSA-N

SMILES: B(C1=CC=C(C2N(C3=CC=CC=C3)C3=CC=CC=C3N=2)C=C1)(O)O

?? ? ?? ??
?? ? ???? ?? (GHS)

HS ??	2933.99.9701

????(GHS):

?? ?:

Warning

??·?? ??:

??	??·?? ??	?? ??	??	?? ?	?? ??	P- ??
H315	??? ??? ???	????? ?? ?????	?? 2	??		P264, P280, P302+P352, P321,P332+P313, P362
H319	?? ?? ??? ???	?? ? ?? ?? ??? ??	?? 2A	??		P264, P280, P305+P351+P338,P337+P313P

??????:

P264	?? ??? ?? ??? ????.
P264	?? ??? ?? ??? ????.
P280	????/???/???/?????? ?????.
P302+P352	??? ??? ??? ?? ????.
P305+P351+P338	?? ??? ? ?? ?? ???? ????. ???? ?????? ?????. ?? ????.
P321	(…) ??? ???.
P332+P313	?? ??? ??? ???? ??· ??? ????.
P362	??? ??? ?? ?? ?? ?????

NFPA 704

	0
1		0

???,B-[4-(1-??-1H-??????-2-?)??]- C??? ??, ??, ??

??? ??

White to off-white powder

Synthesis

The 7g 2 - (4-bromophenyl) - 1-phenyl-benzimidazole (0.02mole) adding 150mlTHF in, lower the temperature to -78 °C, at -78 ° C dropping under 12 ml (2.5M/L, 0 . 03mole) n-BuLi, thermal insulation 30 minutes, dropping 4.26g (0.041mole) methyl borate, reaction 2 hours after the reaction end of the water in the reaction solution of 50 ml, stirring 20 minutes, hydrochloric acid to adjust pH value to acidity, stirring 30 minutes, the reaction solution with ethyl acetate extraction three times, washing time combined with the organic layer, the organic phase is separated, turns on lathe does, solid with petroleum ether heat two times, filtering, to obtain solid intermediates kind of white 4-(1-Phenyl-1H-benzimidazol-2-yl)phenylboronic acid, yield 65percent.

???,B-[4-(1-??-1H-??????-2-?)??]- ?? ?? ? ???

???

2-(4-?????)-1-??-1H-?????? ?????????????? ?????? ? ????????? ????? ????

?? ??

9-Phenyl-3-[4-(1-phenyl-1H-benzimidazol-2-yl)phenyl]-9H-carbazole

???,B-[4-(1-??-1H-??????-2-?)??]- ?? ??

???( 157)?? ??

???	??	???	??	?? ?	??
Henan Fengda Chemical Co., Ltd	+86-371-86557731 +86-13613820652	info@fdachem.com	China	20111	58
Springchem New Material Technology Co.,Limited	+86-021-62885108	info@spring-chem.com	China	2068	57
ATK CHEMICAL COMPANY LIMITED	+undefined-21-51877795	ivan@atkchemical.com	China	32998	60
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BAYNOE CHEM CO.,LTD	+86-21-34783353 +8615000719740	baynoe@baynoe.com	CHINA	934	58
CONIER CHEM AND PHARMA LIMITED		sales@conier.com	China	49906	58

???,B-[4-(1-??-1H-??????-2-?)??]- ?? ??:

4-(1-Phenyl-1H-benzimidazol-2-yl)phenylboronic acid 1,2-Diphenyl-1H-benzimidazole

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