(????????)???????? ?????
|
|
(????????)???????? ????? ??
- ???
- 145-150 °C (dec.) (lit.)
- ?? ??
- Inert atmosphere,Room Temperature
- ???
- ?????(?? ???), ???(?? ???)
- ??? ??
- ??? ??
- ??
- ???
- ???
- ?? ?????.
- ??
- Hygroscopic
- BRN
- 3581273
- InChI
- 1S/C22H22O2P.BrH/c1-2-24-22(23)18-25(19-12-6-3-7-13-19,20-14-8-4-9-15-20)21-16-10-5-11-17-21;/h3-17H,2,18H2,1H3;1H/q+1;/p-1
- InChIKey
- VJVZPTPOYCJFNI-UHFFFAOYSA-M
- SMILES
- [Br-].CCOC(=O)C[P+](c1ccccc1)(c2ccccc2)c3ccccc3
- CAS ??????
- 1530-45-6(CAS DataBase Reference)
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- ?? ? ?? ??
- ?? ? ???? ?? (GHS)
| ??? ?? | Xi | ||
|---|---|---|---|
| ?? ???? ?? | 36/37/38 | ||
| ????? | 26-36-24/25 | ||
| WGK ?? | 3 | ||
| RTECS ?? | TA2299500 | ||
| F ?????? | 9 | ||
| HS ?? | 29310095 | ||
| ???? ??? | 11 - Combustible Solids |
(????????)???????? ????? C??? ??, ??, ??
??? ??
WHITE CRYSTALLINE POWDER??
suzuki reactionPurification Methods
Wash it with pet ether (b 40-50o) and recrystallise it from CHCl3/Et2O and dry it in a high vacuum at 65o. [Isler et al. Helv Chim Acta 40 1242 1957, Wittig & Haag Chem Ber 88 1654, 1664 1955.](????????)???????? ????? ?? ?? ? ???
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DICHLOROTRIPHENYLPHOSPHORANE
Triphenylphosphine hydrobromide
Vecuronium bromide
Rocuronium bromide