ChemicalBook >?? ???? >2-???????-4-?
2-???????-4-?
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2-???????-4-? ??
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- 125-127 °C(lit.)
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- 389.4±42.0 °C(Predicted)
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- 1.269±0.06 g/cm3(Predicted)
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- ?? ? ???? ?? (GHS)
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Purification Methods
This yellow solid is purified by passage through a silica gel column, eluting with *C6H6/Me6CO, evaporating and crystallising the residue from EtOH. The sulfoxide [65373-82-2] has m 133-135o, and the sulfone [22810-82-2] has m 136.5-137o (from EtOH). The dimethylhydrazone has m 111-113o (from BuOH). It forms easily hydrolysable salts. [Nakazumi et al. J Heterocycl Chem 21 193 1984, Chen et al. J Org Chem 51 3282 1986, Van Allen & Reynolds J Heterocycl Chem 8 807 1971, Beilstein 17 I 204, 17 III/IV 5420, 17/10 V 560.]2-???????-4-? ?? ?? ? ???
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| ??? | ?? | ??? | ?? | ?? ? | ?? |
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| Shanghai Haohong Scientific Co., Ltd. | 400-8210725 4008210725 |
malulu@leyan.com | China | 39546 | 58 |




