132-32-1

3-氨基-9-乙基咔唑(132-32-1)核磁圖(¹HNMR)

產(chǎn)品名稱(chēng):3-氨基-9-乙基咔唑

CAS:132-32-1

分子式:C14H14N2

分子量: 210.27

InChI:InChI=1S/C14H14N2/c1-2-16-13-6-4-3-5-11(13)12-9-10(15)7-8-14(12)16/h3-9H,2,15H2,1H3

InChIKey: OXEUETBFKVCRNP-UHFFFAOYSA-N

Smiles:N1(CC)C2=C(C=CC=C2)C2=C1C=CC(N)=C2

¹HNMR

¹³CNMR

IR1

Mass

MS-NW-8137          
3-amino-9-ethylcarbazole
C14H14N2            (Mass of molecular ion:    210)

   Source Temperature: 160 °C
   Sample Temperature: 140 °C
   Direct, 75 eV

      18.0       3.0
      45.0       1.5
      51.0       1.0
      63.0       1.0
      75.0       1.0
      77.0       2.1
      83.5       1.0
      91.0       2.6
      97.5       1.1
     101.0       1.0
     105.0       2.9
     106.0       1.0
     126.0       1.1
     127.0       4.0
     128.0       2.1
     139.0       1.1
     140.0       1.4
     151.0       1.7
     152.0       1.9
     153.0       2.5
     154.0       3.8
     166.0       1.6
     167.0       5.2
     168.0       1.6
     178.0       2.2
     179.0       1.8
     180.0       3.0
     181.0      15.3
     182.0       3.0
     193.0       1.3
     194.0       2.1
     195.0      73.7
     196.0      11.1
     209.0       7.0
     210.0     100.0
     211.0      16.1
     212.0       1.2

90 MHz in CDCl3

¹H NMR	89.56 MHz
C₁₄ H₁₄ N₂	0.044 g : 0.5 ml CDCl₃
3-amino-9-ethylcarbazole

    Assign.     Shift(ppm)

      A             7.948
      B             7.44
      C             7.37
      D             7.15
      E             7.31
      F             7.10
      G             6.862
      J             4.228
      K             3.40
      L             1.338

     Hz     ppm     Int.

    716.00   7.995    218
    708.44   7.911    261
    671.50   7.498     76
    670.50   7.487     82
    666.94   7.447     65
    661.38   7.385    421
    659.00   7.359    443
    656.31   7.329    607
    651.00   7.269    114
    648.44   7.241    174
    645.38   7.207    379
    643.38   7.184    264
    637.50   7.119    564
    631.31   7.050    153
    629.31   7.027    126
    618.69   6.909    224
    617.00   6.890    222
    610.38   6.816    136
    608.50   6.795    132
    389.88   4.354    149
    382.56   4.272    454
    375.44   4.193    481
    368.38   4.114    178
    304.81   3.404    513
    126.88   1.417    522
    122.94   1.373    107
    119.75   1.338   1000
    112.56   1.257    475
    108.69   1.214     71
    108.13   1.208     68

in CDCl3