4-(PYRID-2-YLOXY)BENZALDEHYDE

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Company Name: Hefei Lbao Physical & Chemical Science Co.,Ltd
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Products Intro: Product Name:4-(Pyridin-2-yloxy)benzaldehyde
CAS:194017-69-1
Purity:98% Package:1kg;
Company Name: Shanghai Rlavie Technology Co ltd
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Products Intro: Product Name:4-(Pyridin-2-yloxy)benzaldehyde
CAS:194017-69-1
Purity:98%min Package:1KG;0.00;USD
Company Name: Career Henan Chemica Co
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Products Intro: Product Name:4-(PYRID-2-YLOXY)BENZALDEHYDE
CAS:194017-69-1
Purity:0.99, AD68 Package:1g;1USD
Company Name: Labnetwork lnc.
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Products Intro: Product Name:4-pyridin-2-yloxybenzaldehyde
CAS:194017-69-1
Purity:95% Package:100g; 1kg Remarks:LN01359493
Company Name: Amadis Chemical Company Limited
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Products Intro: Product Name:4-(Pyrid-2-yloxy)benzaldehyde
CAS:194017-69-1
Purity:0.97 Package:mgs,gs,kgs Remarks:A813688

4-(PYRID-2-YLOXY)BENZALDEHYDE manufacturers
4-(PYRID-2-YLOXY)BENZALDEHYDE Basic information
Product Name:4-(PYRID-2-YLOXY)BENZALDEHYDE
Synonyms:4-(PYRID-2-YLOXY)BENZALDEHYDE;4-(Pyridin-2-yloxy)benzaldehyde 97%;4-(2-Pyridyloxy)benzaldehyde;4-(2-Pyridinyloxy)-benzaldehyde;2-(4-Formylphenoxy)pyridine;4-[(Pyridin-2-yl)oxy]benzaldehyde 97+%;Benzaldehyde, 4-(2-pyridinyloxy)-;4-(Pyridin-2-yloxy)benzaldehyde
CAS:194017-69-1
MF:C12H9NO2
MW:199.21
EINECS:
Product Categories:
Mol File:194017-69-1.mol
4-(PYRID-2-YLOXY)BENZALDEHYDE Structure
4-(PYRID-2-YLOXY)BENZALDEHYDE Chemical Properties
Melting point 45 °C
Boiling point 344.8±22.0 °C(Predicted)
density 1+-.0.06 g/cm3(Predicted)
storage temp. under inert gas (nitrogen or Argon) at 2-8°C
form solid
pka2.43±0.12(Predicted)
color Yellow
CAS DataBase Reference194017-69-1
Safety Information
Hazard Codes Xi
Hazard Note Irritant
HS Code 2933399990
MSDS Information
4-(PYRID-2-YLOXY)BENZALDEHYDE Usage And Synthesis
Synthesis
2-Chloropyridine

109-09-1

4-Hydroxybenzaldehyde

123-08-0

4-(PYRID-2-YLOXY)BENZALDEHYDE

194017-69-1

2-Chloropyridine (1) (0.002 mol) and p-hydroxybenzaldehyde (2) (0.002 mol) were added with potassium carbonate (0.002 mol) and 10 mL of anhydrous dimethylformamide (DMF) in a round bottom flask, and the reaction was heated for 3-4 hours at 70°C. After completion of the reaction, the mixture was concentrated under reduced pressure, poured into water and extracted with ethyl acetate. The organic phases were combined, washed with water and dried over anhydrous sodium sulfate. Purification by column chromatography (silica gel G, unfolding agent was ethyl acetate:ethanol=3:2) gave the target product 4-(pyridin-2-yloxy)benzaldehyde in 66.8% yield. The product was detected by TLC (Rf 0.65, iodine vapor color development) showed a single spot, melting point 79-81 ℃, molecular weight 199.21.

References[1] Asian Journal of Chemistry, 2018, vol. 30, # 10, p. 2193 - 2200
[2] Patent: WO2006/31764, 2006, A2. Location in patent: Page/Page column 10-12
4-(PYRID-2-YLOXY)BENZALDEHYDE Preparation Products And Raw materials
Raw materials2-Chloropyridine-->4-Hydroxybenzaldehyde-->N,N-Dimethylformamide-->Potassium carbonate
Tag:4-(PYRID-2-YLOXY)BENZALDEHYDE(194017-69-1) Related Product Information
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