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| | Hexadecyl 3-amino-4-chlorobenzoate Basic information |
| Product Name: | Hexadecyl 3-amino-4-chlorobenzoate | | Synonyms: | 3-AMINO-4-CHLORO BENZOIC ACID HEXADECYL ESTER;HEXADECYL 3-AMINO-4-CHLOROBENZOATE;3-Amino-4-chloro benzoic hexadecyl ester;3-AMINO-4-CHLOROBENZOICACIDHEXADECYLESTERAPPEARANCE;Hexadecylester, 3-Amino-4-chloro benzoate;3-Amino-4-chlorobenzoic acid hexadecyl ester in stock Factory;Benzoic acid, 3-amino-4-chloro-, hexadecyl ester | | CAS: | 143269-74-3 | | MF: | C23H38ClNO2 | | MW: | 396.01 | | EINECS: | 419-700-6 | | Product Categories: | Organic acids | | Mol File: | 143269-74-3.mol |  |
| | Hexadecyl 3-amino-4-chlorobenzoate Chemical Properties |
| Hazard Codes | N | | Risk Statements | 51/53 | | Safety Statements | 61 | | TSCA | TSCA listed |
| | Hexadecyl 3-amino-4-chlorobenzoate Usage And Synthesis |
| Chemical Properties | White to light brown crystalline powder | | Synthesis | A mixture of 16.3 g (0.132 moles) 45percent potassium hydroxide solution, 21.5 g (0.125 moles) of 3-amino-4-chlorobenzoic acid, 100 g of xylene, 40/3 g (0.132 moles) of 1-bromohexadecane and 4.5 g of benzyltriethylammonium bromide (10 mol percent) was heated to reflux. Water was removed using a Dean-Stark trap. After 3 hr at reflux (115-120° C.), the reaction was judged complete by tic. The reaction was cooled to 90° C. and washed with water to remove salts. The solvent was removed on a roto-vap, and the residue was crystallized from heptane to give 40.7 g (83 per cent yield) of a solid Hexadecyl 3-amino-4-chlorobenzoate. | | References | [1] Patent: US2006/135807, 2006, A1. Location in patent: Page/Page column 3
[2] Patent: US2006/135807, 2006, A1. Location in patent: Page/Page column 2 |
| | Hexadecyl 3-amino-4-chlorobenzoate Preparation Products And Raw materials |
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