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| | 2-Methyl-6-quinolinecarbaldehyde Basic information |
| | 2-Methyl-6-quinolinecarbaldehyde Chemical Properties |
| Melting point | 96-99 | | Boiling point | 315.6±22.0 °C(Predicted) | | density | 1.183±0.06 g/cm3(Predicted) | | storage temp. | under inert gas (nitrogen or Argon) at 2-8°C | | form | Solid | | pka | 4.97±0.43(Predicted) | | color | Yellow |
| | 2-Methyl-6-quinolinecarbaldehyde Usage And Synthesis |
| Synthesis | 0.005 mmol of transition metal catalyst was accurately weighed and added to a 10 mL Young reaction tube equipped with a magnetic stirrer. Under oxygen atmosphere, 0.04 mmol of co-catalyst I, 0.08 mmol of co-catalyst II, 0.2 mmol of 4-formylaniline and 1 mL of anhydrous ethanol were added sequentially to the reaction tube. The Young reaction tube was placed on a magnetic stirrer and the reaction was stirred at 150 °C for 30 hours. After completion of the reaction, the pH of the reaction mixture was adjusted to neutral, and 2-methyl-6-formylquinoline was obtained in pure form in 75% yield after post-processing. | | References | [1] Patent: CN106543078, 2017, A. Location in patent: Paragraph 0099; 0100 |
| | 2-Methyl-6-quinolinecarbaldehyde Preparation Products And Raw materials |
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