Product Details
| Product Name: 3-Methyl-4-nitrobenzoic acid | CAS No.: 3113-71-1 |
| Min. Order: 1KG | Purity: 99% |
| Supply Ability: g-kg-tons, free sample is available | Release date: 2025/09/25 |
| Lead time: In stock | Packaging: bottle/ drum/ bucket/ IBC, as request. |
| Delivery: By sea, by air, by express | Origin: Manufacturer |
1. Product information
| Product Name: | 3-Methyl-4-nitrobenzoic acid |
| Synonyms: | 3-METHYL-4-NITROBENZOIC ACID FOR SYNTHES;Methyl-4-nitrobenzoic;3-Methyl-4-nitronbenzoic acid;5-Carboxy-2-nitrotoluene, 4-Nitro-m-toluic acid;3-methyl-4-nitro-benzoicaci;Benzoic acid, 3-methyl-4-nitro-;m-Toluic acid, 4-nitro-;4-NITRO-3-METHYLBENZOIC ACID |
| CAS: | 3113-71-1 |
| MF: | C8H7NO4 |
| MW: | 181.15 |
| EINECS: | 221-479-4 |
| Product Categories: | Aromatic Carboxylic Acids, Amides, Anilides, Anhydrides & Salts;Benzoic acid;Organic acids;pharmaceutical intermediates |
| Mol File: | 3113-71-1.mol |
 | |
| 3-Methyl-4-nitrobenzoic acid Chemical Properties |
| Melting point | 216-218 °C (lit.) |
| Boiling point | 314.24°C (rough estimate) |
| density | 1.4283 (rough estimate) |
| refractive index | 1.5468 (estimate) |
| storage temp. | Sealed in dry,Room Temperature |
| solubility | slightly sol. in Alcohol |
| pka | 3.49±0.10(Predicted) |
| form | Amorphous Powder |
| color | Yellow |
| 3-Methyl-4-nitrobenzoic acid Usage And Synthesis |
| Chemical Properties | white to light yellow crystal powder |
| Uses | 3-Methyl-4-nitrobenzoic Acid is used as a reagent in the synthesis of influenza neuraminidase inhibitors with pyrrolidinobenzoic acid scaffold containing lipophilic side chains. |
| Preparation | 3-Methyl-4-nitrobenzoic acid was synthesized via oxidation of 2,4-(dimethylnitrobenzene) with mole-(cular) oxygen catalyzed by cobalt acetate in acetic acid in the presence of an initiator.It was found that the yield of 3-methyl-4-nitrobenzoic acid increased remarkably with the addition of sodium bromide as a co-(catalyst).The reaction was carried out at 130 ℃ for 8 h at 0.8 MPa of oxygen in the presence of 0.017 mol of cobalt acetate,(0.017 mol) of sodium bromide,and 0.30 mol of 2-butanone with 1.00 mole of 2,4-dimethylnitrobenzene.(Under) these conditions 99% of the reactant converted with a selectivity of 52% to 3-methyl-4-(nitrobenzoic) acid,and the yield of 3methyl-4-(nitrobenzoic) acid was 51%.The reaction mechanism and the function of(sodium) bromide were discussed.According to the fact that the reaction could not proceed without the presence of an initiator,it was proposed that the reaction took place via a free radical mechanism,and(sodium) bromide reacted with Co(Ⅲ) to generate bromine radicals,which promoted the formation of benzyl radicals. Synthesis of 3-Methyl-4-nitrobenzoic Acid via Catalytic Oxidation with Molecular Oxygen Method for preparing 3-methyl-4-nitrobenzoic acid by oxidizing with nitric acid |
| General Description | Needles or off white powder. |
| Air & Water Reactions | Insoluble in water. |
2. Packaging
For powders: normal is 25kgs/Drum or bag, or larger/smaller package as request.
For liquids: normal 25kgs/drum, 180-300kgs/bucket, or IBC, determined by the nature of the product.
Or smaller package 1kg/bottle, 10kgs/bottle as request.
3. Shipping
4. Contact information
For more details, pls contact us freely.
Email address : elin@fdachem.com
Mob: 86 13613820652
WhatsApp/Skype/Wechat/LINE: 86 13613820652
Company Profile Introduction
Henan Fengda Chemical Co., Ltd. a research customization and supplier specializing in PPb grade ultra-high purity electronic chemicals, deeply rooted in the semiconductor and new display fields, committed to providing the most core and purest chemical components for photoresist and high-end display materials.
We provide key monomers for KrF/ArF photoresist, photoacid generators (PAGs), photoacids, and etching solution raw materials, providing cornerstone materials for advanced process photoresist formulations;
We take ICP-MS full spectrum metal impurity analysis as the quality cornerstone and provide ICP-MS metal impurity COA reports to meet the strict industry requirements for PPb grade electronic chemical materials. The COA report contains important data such as NA, Mg, K, Ca, Al, Cr, Fe, Ni, Cu, Zn, Pb, Ag, etc. To provide customers with pure and reliable source assurance for cutting-edge research and stable production.
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