2272-45-9

BENZAL-P-TOLUIDINE(2272-45-9) ¹³C NMR

Product NameBENZAL-P-TOLUIDINE

CAS 2272-45-9

Molecular FormulaC14H13N

Molecular Weight195.26

InChIInChI=1S/C14H13N/c1-12-7-9-14(10-8-12)15-11-13-5-3-2-4-6-13/h2-11H,1H3

InChIKey MSFVFFZPHJPOHP-UHFFFAOYSA-N

SmilesC1(N=CC2=CC=CC=C2)=CC=C(C)C=C1

Request For Quotation

BENZAL-P-TOLUIDINE(2272-45-9) <sup>13</sup>C NMR
Mass

MS-NW-6241          
N-benzylidene-p-toluidine
C14H13N             (Mass of molecular ion:    195)

   Source Temperature: 260 °C
   Sample Temperature: 190 °C
   Reservoir, 75 eV

      27.0       1.3
      38.0       1.0
      39.0       7.4
      41.0       2.3
      50.0       2.2
      51.0       5.7
      52.0       1.6
      62.0       1.3
      63.0       5.4
      64.0       2.1
      65.0      17.1
      66.0       1.1
      76.0       1.5
      77.0       5.3
      78.0       4.1
      83.5       2.8
      89.0       8.1
      90.0       6.1
      91.0      36.3
      92.0       3.3
      95.5       1.5
      96.5       5.3
      97.0       1.0
     106.0       1.1
     116.0       2.3
     117.0       2.1
     118.0      13.0
     119.0       1.4
     152.0       1.6
     165.0       1.6
     167.0       1.0
     180.0       2.5
     192.0       1.1
     193.0       2.5
     194.0      79.9
     195.0     100.0
     196.0      14.9
     197.0       1.2

400 MHz in CDCl3

BENZAL-P-TOLUIDINE(2272-45-9) <sup>13</sup>C NMR

¹H NMR	399.65 MHz
C₁₄ H₁₃ N	0.039 g : 0.5 ml CDCl₃
N-benzylidene-p-toluidine

    Assign.     Shift(ppm)

      A             8.446
      B             7.882
      C             7.45
      D             7.181
      E             7.138
      F             2.355

     Hz     ppm     Int.

   3375.37   8.446    441
   3158.69   7.904     30
   3157.23   7.900     35
   3155.27   7.896    177
   3152.83   7.889    186
   3150.63   7.884    150
   3149.29   7.881    215
   3146.97   7.875    127
   3145.63   7.871    185
   2982.91   7.464     69
   2979.25   7.455    441
   2976.32   7.448    395
   2974.85   7.444    212
   2972.66   7.439    311
   2970.21   7.433     86
   2875.61   7.196    178
   2867.43   7.175    385
   2857.06   7.149    105
   2855.22   7.145    495
   2853.03   7.139    156
   2848.88   7.129     88
   2846.80   7.124    216
    941.28   2.356   1000

in CDCl3