50816-20-1

1-BROMO-8-(TETRAHYDROPYRANYLOXY)OCTANE(50816-20-1) ¹³C NMR

Product Name1-BROMO-8-(TETRAHYDROPYRANYLOXY)OCTANE

CAS 50816-20-1

Molecular FormulaC13H25BrO2

Molecular Weight293.24

InChIInChI=1S/C13H25BrO2/c14-10-6-3-1-2-4-7-11-15-13-9-5-8-12-16-13/h13H,1-12H2

InChIKey JCRBYQZIJFWGOO-UHFFFAOYSA-N

SmilesC1(OCCCCCCCCBr)OCCCC1

Request For Quotation

¹HNMR

¹³CNMR

IR1

1-BROMO-8-(TETRAHYDROPYRANYLOXY)OCTANE(50816-20-1) <sup>13</sup>C NMR
Mass

MS-NW-6120          
2-(8-bromooctyloxy)tetrahydropyran
C13H25BrO2          (Mass of molecular ion:    292)

   Source Temperature: 250 °C
   Sample Temperature: 190 °C
   Reservoir, 75 eV

      27.0       7.9
      28.0       4.2
      29.0      10.8
      31.0       3.9
      39.0       5.3
      40.0       1.2
      41.0      27.2
      42.0       4.6
      43.0      10.7
      44.0       1.6
      53.0       2.1
      54.0       3.6
      55.0      27.6
      56.0      29.5
      57.0      16.4
      67.0       7.0
      68.0       4.0
      69.0      28.3
      70.0       2.5
      71.0       2.8
      81.0       1.9
      82.0       2.4
      83.0       6.0
      84.0       9.1
      85.0     100.0
      86.0       6.4
     101.0       6.5
     102.0       1.2
     111.0       6.2
     115.0       1.8
     135.0       2.5
     137.0       2.2
     148.0       2.0
     149.0       1.2
     150.0       2.1
     151.0       1.2
     162.0       1.7
     164.0       1.6
     191.0       1.0
     193.0       1.0
     291.0       1.0
     293.0       1.0

400 MHz in CDCl3

1-BROMO-8-(TETRAHYDROPYRANYLOXY)OCTANE(50816-20-1) <sup>13</sup>C NMR

¹H NMR	399.65 MHz
C₁₃ H₂₅ Br O₂	0.04 ml : 0.5 ml CDCl₃
2-(8-bromooctyloxy)tetrahydropyran

    Assign.     Shift(ppm)

      A             4.574
      B             3.870
      C             3.730
      D             3.505
      E             3.405
      F             3.383
      G             1.853
      J             1.71
      K          1.59 to 1.55
      L             1.43
      M             1.34

     Hz     ppm     Int.

   1831.79   4.584    152
   1829.10   4.577    230
   1827.39   4.573    169
   1824.58   4.566    166
   1546.51   3.870    140
   1496.09   3.744    234
   1493.41   3.737    138
   1489.26   3.727    132
   1486.57   3.720    258
   1479.61   3.703    129
   1367.80   3.423    501
   1362.06   3.409    288
   1360.84   3.406   1000
   1356.20   3.394    316
   1354.00   3.388    559
   1349.61   3.377    165
   1346.68   3.370    240
    747.68   1.871    301
    740.60   1.854    361
    734.62   1.839    212
    732.91   1.834    321
    726.07   1.817    204
    683.11   1.710    136
    644.78   1.614    183
    644.53   1.613    183
    643.19   1.610    190
    636.72   1.594    323
    635.86   1.592    309
    631.23   1.580    315
    627.44   1.570    205
    623.78   1.561    250
    619.51   1.551    244
    617.68   1.546    276
    616.70   1.544    287
    614.14   1.537    292
    608.52   1.523    179
    607.54   1.521    169
    605.96   1.517    141
    571.17   1.430    189
    535.16   1.340    700

in CDCl3