ALPHA-(CYANOIMINO)-3,4-DICHLOROPHENETHYL -AMINE, 99%(55770-03-1) 13C NMR
Product NameALPHA-(CYANOIMINO)-3,4-DICHLOROPHENETHYL -AMINE, 99%
CAS55770-03-1
Molecular FormulaC9H7Cl2N3
Molecular Weight228.08
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MassMS-NW-9999 alpha-cyanoimino-3,4-dichlorophenethylamine C9H7Cl2N3 (Mass of molecular ion: 227)
Source Temperature: 200 °C Sample Temperature: 140 °C Direct, 75 eV
18.0 4.2 27.0 1.3 28.0 5.3 36.0 2.4 37.0 1.3 38.0 2.0 39.0 4.6 41.0 3.1 42.0 23.6 43.0 20.8 44.0 1.3 49.0 1.3 50.0 3.6 51.0 2.3 56.5 1.2 57.5 1.8 61.0 3.2 61.5 1.4 62.0 5.8 63.0 10.1 64.0 1.8 68.0 34.8 69.0 1.2 72.0 1.0 73.0 7.6 74.0 4.3 74.5 1.9 75.0 6.5 75.5 2.2 76.0 1.5 82.0 1.0 84.0 1.7 85.0 2.3 86.0 2.6 87.0 4.5 88.0 3.4 89.0 15.0 90.0 1.8 92.5 1.0 95.5 1.4 96.0 1.4 97.0 3.6 99.0 4.9 100.0 1.3 101.0 1.7 102.0 1.1 107.0 1.0 109.0 3.0 111.0 1.8 114.0 5.7 115.0 2.3 116.0 1.2 123.0 23.5 124.0 8.8 125.0 19.5 126.0 3.8 127.0 4.2 129.0 1.0 133.0 3.9 135.0 2.6 148.0 1.4 149.0 1.3 150.0 78.9 151.0 11.0 152.0 26.3 153.0 3.6 156.0 1.2 157.0 2.8 158.0 1.2 159.0 73.2 160.0 11.1 161.0 50.1 162.0 7.0 163.0 10.1 164.0 1.5 165.0 3.6 167.0 1.0 184.0 3.3 185.0 51.8 186.0 27.0 187.0 63.7 188.0 18.9 189.0 25.1 190.0 4.3 191.0 4.3 192.0 3.2 194.0 1.0 199.0 1.2 200.0 8.8 201.0 2.4 202.0 5.8 203.0 1.2 204.0 1.0 210.0 3.4 212.0 2.2 226.0 10.0 227.0 100.0 228.0 19.4 229.0 64.3 230.0 9.3 231.0 10.6 232.0 1.3
400 MHz in DMSO-d6 (at 50.C)
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1H NMR 399.65 MHz C9 H7 Cl2 N3 0.041 g : 0.5 ml DMSO-d6 at 50C alpha-cyanoimino-3,4-dichlorophenethylamine 
Assign. Shift(ppm)
A *1 8.5 B *1 8.4 C 7.60 D 7.60 E 7.33 F 3.71 J(C,E)=8.2HZ
Hz ppm Int.3338.01 8.353 124 3056.95 7.650 28 3056.49 7.648 30 3055.27 7.645 34 3052.98 7.640 40 3052.52 7.638 41 3052.06 7.637 43 3042.76 7.614 655 3034.52 7.593 1000 3022.61 7.564 34 3020.78 7.559 27 2942.20 7.362 33 2932.74 7.339 295 2932.28 7.338 295 2924.80 7.319 259 2924.35 7.318 259 1480.71 3.706 189
in DMSO-d6 (at 80.C)
KBr disc
nujol mull
