59146-96-2

2,3-DIMETHYL-6-NITROANILINE(59146-96-2) ¹³C NMR

Product Name2,3-DIMETHYL-6-NITROANILINE

CAS 59146-96-2

Molecular FormulaC8H10N2O2

Molecular Weight166.18

InChIInChI=1S/C8H10N2O2/c1-5-3-4-7(10(11)12)8(9)6(5)2/h3-4H,9H2,1-2H3

InChIKey YEFYPFWBLCARLC-UHFFFAOYSA-N

SmilesC1(N)=C([N+]([O-])=O)C=CC(C)=C1C

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2,3-DIMETHYL-6-NITROANILINE(59146-96-2) <sup>13</sup>C NMR
Mass

MS-NW-7016          
6-nitro-2,3-xylidine
C8H10N2O2           (Mass of molecular ion:    166)

   Source Temperature: 180 °C
   Sample Temperature: 110 °C
   Direct, 75 eV

      18.0       1.9
      27.0       5.0
      28.0       7.1
      30.0       2.2
      38.0       2.5
      39.0      11.4
      40.0       1.6
      41.0       5.4
      42.0       6.7
      50.0       3.0
      51.0       8.2
      52.0       7.0
      53.0       7.3
      54.0       4.4
      58.5       1.7
      62.0       1.5
      63.0       4.3
      64.0       2.1
      65.0      11.6
      66.0       4.1
      67.0       2.5
      75.0       1.2
      76.0       1.7
      77.0      24.3
      78.0       6.2
      79.0       4.8
      80.0       3.5
      81.0       1.1
      89.0       2.6
      90.0       2.4
      91.0      21.7
      92.0       5.5
      93.0      14.2
      94.0       4.1
     102.0       1.5
     103.0       9.3
     104.0      14.0
     105.0       5.9
     106.0       2.3
     107.0       1.0
     108.0       6.8
     116.0       2.2
     117.0       4.2
     118.0      13.9
     119.0      18.8
     120.0      29.7
     121.0       3.8
     129.0       1.5
     130.0       4.7
     131.0       5.9
     132.0       1.1
     133.0       2.1
     136.0       7.2
     148.0       1.9
     149.0      10.6
     150.0       2.6
     151.0       1.8
     165.0       1.6
     166.0     100.0
     167.0      10.3

400 MHz in CDCl3

2,3-DIMETHYL-6-NITROANILINE(59146-96-2) <sup>13</sup>C NMR

¹H NMR	399.65 MHz
C₈ H₁₀ N₂ O₂	0.041 g : 0.5 ml CDCl₃
6-nitro-2,3-xylidine

    Assign.     Shift(ppm)

      A             7.902
      B             6.524
      C             6.
      D     *1      2.304
      E     *1      2.112

     Hz     ppm     Int.

   3162.84   7.915    163
   3154.05   7.893    170
   2611.94   6.536    184
   2611.57   6.535    172
   2603.15   6.514    180
   2602.66   6.513    167
    920.90   2.305   1000
    844.36   2.113    971

in CDCl3