938-71-6

4-CHLORO-2-NITROBENZYL CHLORIDE(938-71-6) ¹³C NMR

Product Name4-CHLORO-2-NITROBENZYL CHLORIDE

CAS 938-71-6

Molecular FormulaC7H5Cl2NO2

Molecular Weight206.03

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4-CHLORO-2-NITROBENZYL CHLORIDE(938-71-6) <sup>13</sup>C NMR
Mass

MS-IW-0577          
4-chloro-1-chloromethyl-2-nitrobenzene
C7H5Cl2NO2          (Mass of molecular ion:    205)

   Source Temperature: 270 °C
   Sample Temperature: 150 °C
   Reservoir, 75 eV

      29.0       2.4
      30.0       5.9
      36.0       1.1
      37.0       1.9
      38.0       4.2
      39.0      12.1
      44.0       1.0
      49.0       2.7
      50.0      11.2
      51.0      14.2
      52.0       2.4
      60.0       1.1
      61.0       7.4
      62.0      23.7
      63.0      51.5
      64.0       4.9
      65.0       1.2
      72.0       1.9
      73.0      22.7
      74.0       8.1
      75.0      28.5
      76.0      10.7
      77.0      16.8
      78.0      13.8
      79.0       1.8
      83.0       1.0
      84.0       2.0
      85.0       6.8
      86.0       9.9
      87.0      14.2
      88.0       6.5
      89.0      76.4
      90.0      76.6
      91.0      14.9
      92.0       1.1
      96.0       1.3
      97.0      10.3
      98.0       3.1
      99.0      76.7
     100.0       6.0
     101.0      23.9
     102.0       2.8
     106.0       2.8
     107.0       1.9
     109.0       2.5
     110.0       4.3
     111.0      30.6
     112.0      53.4
     113.0      18.4
     114.0      31.3
     115.0       5.4
     116.0       5.1
     117.0       1.1
     123.0      78.5
     124.0      43.4
     125.0      36.3
     126.0      79.1
     127.0       9.0
     128.0      21.6
     129.0       1.8
     133.0      16.6
     134.0       1.4
     135.0      11.0
     137.0       1.9
     138.0       2.0
     139.0      26.8
     140.0      12.3
     141.0      10.0
     142.0      33.0
     143.0       2.8
     144.0       9.7
     145.0       1.0
     146.0       1.6
     148.0       1.0
     152.0       1.7
     153.0       9.3
     154.0       3.8
     155.0       3.8
     156.0       1.2
     158.0       7.7
     159.0      17.4
     160.0      19.9
     161.0      12.4
     162.0      10.5
     163.0       2.6
     164.0       1.6
     170.0     100.0
     171.0       8.5
     172.0      32.5
     173.0       2.9
     205.0       2.4
     207.0       1.5

400 MHz in CDCl3

4-CHLORO-2-NITROBENZYL CHLORIDE(938-71-6) <sup>13</sup>C NMR

¹H NMR	399.65 MHz
C₇ H₅ Cl₂ N O₂	0.035 g : 0.5 ml CDCl₃
4-chloro-1-chloromethyl-2-nitrobenzene

    Assign.     Shift(ppm)

      A             8.064
      B             7.654
      C             7.637
      D             4.942

     Hz     ppm     Int.

   3223.63   8.067    217
   3221.92   8.062    224
   3066.28   7.673     65
   3065.80   7.672     66
   3057.86   7.652    337
   3057.50   7.651    341
   3054.69   7.644    309
   3052.73   7.639    280
   3046.39   7.623     58
   3044.43   7.618     66
   1975.10   4.943   1000

in CDCl3