TRIBUTYL(1-ETHOXYVINYL)TIN(97674-02-7) 13C NMR
Product NameTRIBUTYL(1-ETHOXYVINYL)TIN
CAS97674-02-7
Molecular FormulaC16H34OSn
Molecular Weight361.15
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MassMS-NW-9651 tributyl(1-ethoxyvinyl)stannane C16H34OSn (Mass of molecular ion: 362)
Source Temperature: 260 °C Sample Temperature: 150 °C Reservoir, 75 eV
27.0 3.6 28.0 2.4 29.0 8.4 31.0 1.6 39.0 2.2 41.0 7.8 42.0 1.0 43.0 5.5 44.0 1.4 45.0 1.6 55.0 2.0 56.0 2.9 57.0 4.7 73.0 2.0 116.0 2.5 117.0 10.9 118.0 8.9 119.0 20.0 120.0 12.1 121.0 26.1 122.0 2.3 123.0 9.2 125.0 4.8 127.0 11.4 128.0 1.0 131.0 1.5 132.0 1.0 133.0 2.9 134.0 1.5 135.0 4.0 137.0 1.7 143.0 1.3 145.0 3.3 146.0 1.3 147.0 4.2 148.0 1.2 149.0 4.4 151.0 1.3 159.0 1.6 161.0 9.3 162.0 4.6 163.0 14.6 164.0 5.3 165.0 18.9 167.0 4.3 169.0 3.9 171.0 3.5 172.0 1.0 173.0 10.5 174.0 6.2 175.0 46.0 176.0 24.0 177.0 70.5 178.0 22.6 179.0 75.2 180.0 3.7 181.0 13.5 183.0 13.0 187.0 1.3 189.0 9.4 190.0 5.4 191.0 15.5 192.0 5.7 193.0 18.5 195.0 3.3 197.0 3.8 199.0 2.4 200.0 1.3 201.0 4.3 202.0 1.9 203.0 5.9 204.0 1.1 205.0 2.7 207.0 1.6 219.0 4.7 220.0 2.5 221.0 7.1 222.0 2.8 223.0 8.9 225.0 1.4 227.0 3.2 229.0 1.8 230.0 6.3 231.0 28.8 232.0 24.5 233.0 47.0 234.0 30.7 235.0 58.2 236.0 6.9 237.0 8.6 238.0 3.0 239.0 10.5 240.0 1.0 241.0 3.0 243.0 3.2 244.0 2.0 245.0 44.7 246.0 27.2 247.0 76.3 248.0 32.4 249.0 100.0 250.0 8.9 251.0 15.1 252.0 1.4 253.0 17.9 254.0 1.9 255.0 3.0 256.0 1.6 257.0 4.4 258.0 1.6 259.0 4.5 261.0 1.4 263.0 1.2 275.0 5.2 276.0 3.2 277.0 8.4 278.0 3.8 279.0 10.7 280.0 1.2 281.0 1.7 283.0 2.4 287.0 9.0 288.0 6.2 289.0 15.4 290.0 7.6 291.0 20.3 292.0 2.7 293.0 3.0 295.0 3.6 297.0 2.7 299.0 1.9 300.0 1.3 301.0 39.0 302.0 27.6 303.0 69.2 304.0 35.2 305.0 91.3 306.0 16.5 307.0 13.5 308.0 2.4 309.0 16.3 310.0 3.4 311.0 4.1 312.0 1.9 313.0 5.6 314.0 1.3 315.0 3.7 317.0 1.1
400 MHz in CDCl3
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1H NMR 399.65 MHz C16 H34 O Sn 0.05 ml : 0.5 ml CDCl3 tributyl(1-ethoxyvinyl)stannane 
Assign. Shift(ppm)
A *1 4.672 B *1 4.041 C 3.693 D 1.53 E 1.324 F 1.252 G 0.943 J 0.892
Hz ppm Int.1868.16 4.675 91 1866.46 4.671 95 1616.09 4.044 117 1614.38 4.040 117 1486.33 3.720 51 1479.37 3.702 145 1472.41 3.685 147 1465.45 3.667 51 547.36 1.370 63 540.04 1.352 163 532.71 1.333 227 524.90 1.314 230 517.82 1.296 148 510.62 1.278 58 507.45 1.270 192 500.49 1.253 361 493.53 1.235 184 384.77 0.963 310 382.32 0.957 43 379.15 0.949 132 377.93 0.946 142 376.59 0.943 260 375.12 0.939 172 372.44 0.932 52 368.53 0.923 290 363.65 0.910 550 356.32 0.892 1000 352.66 0.883 55 349.12 0.874 501
in CDCl3
liquid film
