二異丙胺(108-18-9)核磁圖(1HNMR)
InChI:InChI=1S/C6H15N/c1-5(2)7-6(3)4/h5-7H,1-4H3
InChIKey: UAOMVDZJSHZZME-UHFFFAOYSA-N
Smiles:CC(NC(C)C)C
-
Mass
MS-NW-0580
diisopropylamine
C6H15N (Mass of molecular ion: 101)
Source Temperature: 260 °C
Sample Temperature: 150 °C
Reservoir, 75 eV
15.0 2.7
18.0 3.3
27.0 5.4
28.0 4.5
30.0 1.8
39.0 3.4
41.0 8.1
42.0 9.2
43.0 9.2
44.0 100.0
45.0 2.6
56.0 1.6
58.0 8.1
70.0 2.0
86.0 41.8
87.0 2.4
100.0 1.3
101.0 3.8
90 MHz in CDCl3
parameter neat
-
| 1H NMR |
89.56 MHz |
| C6 H15 N
|
0.04 ml : 0.5 ml CDCl3
|
| diisopropylamine
|
 |
Assign. Shift(ppm)
A 2.91
B 1.042
C 1.0
|
Hz ppm Int.
266.88 2.980 47
260.63 2.911 63
254.38 2.841 52
248.19 2.772 24
96.31 1.076 1000
92.75 1.036 35
90.06 1.006 907
-
| 1H NMR |
300 MHz |
| C6 H15 N
|
neat
|
| diisopropylamine
|
|
Parameter ppm Hz
D(A) 2.86
D(B) 1.00
J(A,B) 6.3
D(C) 3.06
RANFT,J. ANN.PHYS. 10, 1 (1962)
|
Hz ppm Int.
918.00 3.060 166
870.71 2.902 29
864.40 2.881 72
858.09 2.860 98
851.80 2.839 76
845.51 2.818 32
303.14 1.010 1000
296.85 0.989 974
OXIDATION WITH PERBENZOIC ACID
AIR OXIDATION IN POLYSTYRENE AND METHANOL
AIR OXIDATION IN PVP CAGE