1191-67-9

1,10-癸二硫醇(1191-67-9)紅外圖譜(IR1)

產(chǎn)品名稱:1,10-癸二硫醇

CAS:1191-67-9

分子式:C10H22S2

分子量: 206.41

InChI:InChI=1S/C10H22S2/c11-9-7-5-3-1-2-4-6-8-10-12/h11-12H,1-10H2

InChIKey: UOQACRNTVQWTFF-UHFFFAOYSA-N

Smiles:C(S)CCCCCCCCCS

¹HNMR

¹³CNMR

IR1

Mass

MS-NW-3798          
1,10-decanedithiol
C10H22S2            (Mass of molecular ion:    206)

   Source Temperature: 280 °C
   Sample Temperature: 180 °C
   Reservoir, 75 eV

      18.0       2.1
      27.0      17.4
      28.0       2.5
      29.0      21.0
      34.0       2.3
      35.0       4.7
      39.0      14.5
      40.0       2.6
      41.0      70.9
      42.0      11.6
      43.0      26.0
      44.0       1.4
      45.0       9.0
      46.0       3.6
      47.0      42.1
      48.0       1.5
      49.0       2.1
      53.0       6.4
      54.0      30.5
      55.0     100.0
      56.0      13.2
      57.0      17.2
      58.0       1.2
      59.0       4.2
      60.0      20.9
      61.0      25.8
      62.0       2.1
      63.0       1.4
      65.0       1.1
      66.0       4.5
      67.0      51.3
      68.0      46.1
      69.0      51.5
      70.0       7.1
      71.0       6.9
      73.0       5.3
      74.0       6.1
      75.0       2.8
      79.0       1.8
      80.0       1.2
      81.0      34.4
      82.0      34.1
      83.0      29.8
      84.0       3.4
      85.0       4.1
      86.0       1.4
      87.0      96.1
      88.0      15.4
      89.0      29.4
      90.0       2.1
      91.0       1.7
      95.0      25.3
      96.0      13.7
      97.0      11.6
      98.0       1.3
     100.0       1.1
     101.0      74.2
     102.0       8.9
     103.0       7.6
     104.0       1.0
     109.0       7.5
     110.0       6.5
     111.0       1.6
     115.0      27.5
     116.0       3.3
     117.0       2.5
     129.0      20.3
     130.0       2.1
     131.0       1.4
     138.0       1.7
     143.0       8.7
     144.0       1.1
     157.0       1.2
     171.0      26.5
     172.0      10.0
     173.0       8.9
     174.0       1.6
     206.0      18.0
     207.0       2.5
     208.0       1.8

90 MHz in CDCl3

¹H NMR	89.56 MHz
C₁₀ H₂₂ S₂	0.04 ml : 0.5 ml CDCl₃
1,10-decanedithiol

    Assign.     Shift(ppm)

      A             2.516
      B             1.60
      C             1.324
      D          1.46 to 1.26

     Hz     ppm     Int.

    236.94   2.646     65
    236.06   2.636     65
    229.38   2.562    228
    222.63   2.486    268
    214.88   2.400    125
    150.94   1.686     68
    150.38   1.680     68
    148.38   1.657     58
    148.00   1.653     57
    143.50   1.603    113
    142.69   1.594    108
    141.75   1.583    112
    138.81   1.550     96
    136.88   1.529    110
    134.56   1.503     85
    130.88   1.462    123
    128.00   1.430    147
    125.81   1.405    464
    123.44   1.379    126
    118.31   1.322    696
    115.00   1.285   1000
    110.50   1.234    328

in CDCl3