123-00-2

N-(3-氨丙基)嗎啉(123-00-2)質(zhì)譜(MS)

產(chǎn)品名稱:N-(3-氨丙基)嗎啉

CAS:123-00-2

分子式:C7H16N2O

分子量: 144.21

InChI:InChI=1S/C7H16N2O/c8-2-1-3-9-4-6-10-7-5-9/h1-8H2

InChIKey: UIKUBYKUYUSRSM-UHFFFAOYSA-N

Smiles:N1(CCCN)CCOCC1

Mass

MS-NW-1362          
3-morpholinopropylamine
C7H16N2O            (Mass of molecular ion:    144)

   Source Temperature: 260 °C
   Sample Temperature: 180 °C
   Reservoir, 75 eV

      15.0       4.4
      18.0       3.0
      26.0       1.0
      27.0       5.3
      28.0      16.2
      29.0       6.6
      30.0      31.6
      31.0       1.7
      39.0       1.5
      41.0       7.3
      42.0      14.7
      43.0      21.8
      44.0      11.6
      45.0       1.9
      54.0       2.9
      55.0       4.5
      56.0      38.6
      57.0      24.1
      58.0       6.7
      59.0       2.3
      68.0       2.1
      69.0       2.7
      70.0      12.1
      71.0       7.6
      72.0       2.8
      82.0       1.8
      83.0       3.4
      84.0       3.4
      85.0       3.5
      86.0       8.4
      87.0       1.7
      88.0       8.6
      96.0       1.4
      97.0       2.0
      98.0       2.5
      99.0       1.0
     100.0     100.0
     101.0      16.2
     102.0       1.0
     112.0       5.9
     113.0      23.4
     114.0       8.1
     126.0       6.8
     127.0       9.7

90 MHz in CDCl3

¹H NMR	89.56 MHz
C₇ H₁₆ N₂ O	0.04 ml : 0.5 ml CDCl₃
3-morpholinopropylamine

    Assign.     Shift(ppm)

      A             3.702
      B             2.750
      C             2.43
      D             2.40
      E             1.637
      F             1.37

     Hz     ppm     Int.

    336.50   3.758    425
    331.94   3.707    379
    330.00   3.685    213
    327.06   3.652    477
    253.63   2.832    192
    246.81   2.756    477
    240.13   2.682    269
    222.69   2.487    572
    220.00   2.457    240
    217.94   2.434    427
    215.63   2.408    460
    213.31   2.382    450
    208.06   2.324    246
    153.19   1.711    134
    152.31   1.701    138
    145.50   1.625    183
    139.06   1.553     98
    138.38   1.546    112
    122.69   1.370   1000

in CDCl3