134-32-7

1-萘胺(134-32-7)核磁圖(¹HNMR)

產(chǎn)品名稱:1-萘胺

CAS:134-32-7

分子式:C10H9N

分子量: 143.19

InChI:InChI=1S/C10H9N/c11-10-7-3-5-8-4-1-2-6-9(8)10/h1-7H,11H2

InChIKey: RUFPHBVGCFYCNW-UHFFFAOYSA-N

Smiles:C1(N)=C2C(C=CC=C2)=CC=C1

Mass

MS-NW-8709          
1-naphthylamine
C10H9N              (Mass of molecular ion:    143)

   Source Temperature: 260 °C
   Sample Temperature: 150 °C
   Reservoir, 75 eV

      39.0       2.1
      50.0       1.1
      51.0       1.6
      57.5       2.2
      58.5       4.1
      62.0       1.4
      63.0       3.2
      65.0       1.7
      70.5       4.8
      71.5       7.8
      74.0       1.1
      75.0       1.2
      76.0       1.1
      77.0       1.4
      88.0       1.1
      89.0       3.8
      90.0       1.1
     113.0       1.6
     114.0       2.4
     115.0      31.0
     116.0      17.9
     117.0       3.2
     126.0       1.3
     140.0       2.0
     141.0       1.0
     142.0       5.3
     143.0     100.0
     144.0      11.3

400 MHz in CDCl3

¹H NMR	399.65 MHz
C₁₀ H₉ N	0.041 g : 0.5 ml CDCl₃
1-naphthylamine

    Assign.     Shift(ppm)

      A             7.77
      B             7.75
      C     *1      7.43
      D     *1      7.40
      E             7.290
      F             7.261
      G             6.716
      J             4.04

     Hz     ppm     Int.

   3115.72   7.797     34
   3111.45   7.786    278
   3109.01   7.780    316
   3107.06   7.775     61
   3105.47   7.771    173
   3103.15   7.765    527
   3102.05   7.762    584
   3100.22   7.758    157
   3099.24   7.755    138
   3095.83   7.747    292
   3094.12   7.743    236
   3093.38   7.741    328
   3089.48   7.731     37
   3088.87   7.729     36
   2976.81   7.449     93
   2975.10   7.445    158
   2969.97   7.432    437
   2968.26   7.428    384
   2966.55   7.423    490
   2963.50   7.416   1000
   2960.45   7.408    409
   2958.62   7.404    386
   2956.79   7.399    418
   2951.78   7.386    149
   2949.95   7.382     96
   2921.02   7.309    108
   2919.56   7.306    165
   2919.19   7.305    154
   2911.62   7.286    499
   2910.89   7.284    438
   2907.47   7.276    818
   2904.66   7.269     30
   2900.51   7.258    734
   2899.29   7.255    259
   2892.33   7.238    294
   2688.35   6.727    475
   2686.89   6.724    463
   2681.52   6.710    464
   2679.93   6.706    464
   1615.48   4.043    112

in CDCl3