14548-44-8

(4-氯苯)(吡啶-3-基)甲酮(14548-44-8)核磁圖(¹HNMR)

產(chǎn)品名稱(chēng):(4-氯苯)(吡啶-3-基)甲酮

CAS:14548-44-8

分子式:C12H8ClNO

分子量: 217.65

Mass

MS-NW-7446          
p-chlorophenyl 3-pyridyl ketone
C12H8ClNO           (Mass of molecular ion:    217)

   Source Temperature: 160 °C
   Sample Temperature: 110 °C
   Direct, 75 eV

      50.0       6.4
      51.0      12.0
      52.0       1.5
      63.0       1.2
      74.0       2.8
      75.0      13.5
      76.0       3.7
      77.0       1.7
      78.0      17.2
      79.0       1.1
      85.0       1.4
     106.0      14.6
     107.0       1.1
     111.0      26.4
     112.0       2.0
     113.0       8.7
     126.0       1.2
     127.0       1.9
     139.0      62.9
     140.0       5.1
     141.0      20.7
     142.0       1.6
     153.0       1.2
     154.0       3.4
     182.0     100.0
     183.0      13.7
     184.0       1.1
     216.0       2.9
     217.0      15.2
     218.0       3.2
     219.0       5.2

90 MHz in CDCl3

¹H NMR	89.56 MHz
C₁₂ H₈ Cl N O	0.037 g : 0.5 ml CDCl₃
p-chlorophenyl 3-pyridyl ketone

    Assign.     Shift(ppm)

      A             8.960
      B             8.804
      C             8.070
      D             7.750
      E             7.50
      F             7.43

     Hz     ppm     Int.

    803.94   8.977    273
    803.31   8.970    289
    801.88   8.954    306
    801.06   8.945    280
    798.75   8.919     58
    792.00   8.844    215
    790.19   8.824    233
    787.13   8.789    239
    785.38   8.770    242
    729.19   8.142    169
    727.38   8.122    213
    727.00   8.118    194
    725.19   8.098    159
    721.25   8.054    220
    719.50   8.034    273
    719.06   8.029    256
    717.31   8.010    194
    701.81   7.837     96
    699.75   7.814    521
    697.63   7.790    218
    696.00   7.772     68
    695.38   7.765     70
    694.94   7.760     75
    693.13   7.740    316
    690.94   7.715    957
    688.94   7.693    201
    686.75   7.669     52
    686.19   7.662     51
    675.94   7.548    220
    674.00   7.526   1000
    672.13   7.505    405
    671.81   7.502    417
    669.63   7.477     98
    667.31   7.451    424
    666.44   7.442    334
    665.69   7.433    438
    665.13   7.427    554
    664.31   7.418    261
    663.38   7.408    232
    659.44   7.364    173
    658.50   7.353    163

in CDCl3