17873-08-4

三甲基(苯硫甲基)硅烷(17873-08-4)核磁圖(¹HNMR)

產(chǎn)品名稱:三甲基(苯硫甲基)硅烷

CAS:17873-08-4

分子式:C10H16SSi

分子量: 196.38

InChI:InChI=1S/C10H16SSi/c1-12(2,3)9-11-10-7-5-4-6-8-10/h4-8H,9H2,1-3H3

InChIKey: UOQDIMYVQSHALM-UHFFFAOYSA-N

Smiles:C1(SC[Si](C)(C)C)=CC=CC=C1

Mass

MS-IW-5092          
trimethyl(phenylthiomethyl)silane
C10H16SSi           (Mass of molecular ion:    196)

   Source Temperature: 210 °C
   Sample Temperature: 150 °C
   Reservoir, 75 eV

      29.0       1.0
      31.0       1.1
      39.0       1.2
      43.0       5.4
      44.0       3.7
      45.0      10.2
      51.0       3.6
      57.0       1.3
      58.0       1.2
      59.0       4.8
      65.0       2.6
      72.0       5.2
      73.0     100.0
      74.0      10.6
      75.0       5.7
      77.0       6.2
      78.0       1.0
      79.0       1.0
      90.5       1.1
      91.0      15.3
      92.0       1.2
     105.0       6.8
     107.0       1.0
     109.0       1.5
     121.0       1.1
     135.0      11.8
     136.0       1.7
     137.0       2.8
     151.0       4.1
     153.0       1.0
     165.0      18.3
     166.0       3.0
     167.0       2.3
     181.0      39.9
     182.0       6.3
     183.0       3.6
     196.0      34.9
     197.0       6.0
     198.0       3.0

400 MHz in CDCl3

¹H NMR	399.65 MHz
C₁₀ H₁₆ S Si	0.05 ml : 0.5 ml CDCl₃
trimethyl(phenylthiomethyl)silane

    Assign.     Shift(ppm)

      A             7.265
      B             7.234
      C             7.072
      D             2.155
      E             0.155

     Hz     ppm     Int.

   2910.64   7.283     53
   2908.94   7.279     72
   2906.98   7.274     33
   2904.17   7.267     55
   2901.98   7.262    191
   2900.63   7.258    170
   2897.58   7.251    167
   2895.14   7.245     38
   2890.38   7.233    146
   2888.55   7.228     66
   2883.91   7.217     33
   2882.08   7.212     64
   2834.47   7.093     31
   2833.01   7.089     53
   2831.30   7.085     30
   2825.93   7.072     70
   2824.83   7.069     38
   2824.10   7.067     30
   2819.09   7.054     37
    864.26   2.163     42
    861.33   2.156    413
     65.06   0.163    244
     61.89   0.155   1000
     58.35   0.147    165

in CDCl3