18295-64-2

10-氯-3-癸炔(18295-64-2)核磁圖(¹HNMR)

產(chǎn)品名稱:10-氯-3-癸炔

CAS:18295-64-2

分子式:C10H17Cl

分子量: 172.7

InChI:InChI=1S/C10H17Cl/c1-2-3-4-5-6-7-8-9-10-11/h2,5-10H2,1H3

InChIKey: BQQIODGRFRSXTM-UHFFFAOYSA-N

Smiles:CCC#CCCCCCCCl

¹HNMR

¹³CNMR

IR1

Mass

MS-IW-9726          
10-chloro-3-decyne
C10H17Cl            (Mass of molecular ion:    172)

   Source Temperature: 220 °C
   Sample Temperature: 150 °C
   Reservoir, 75 eV

      27.0      11.6
      28.0       1.4
      29.0       8.3
      36.0       2.4
      38.0       1.3
      39.0      17.2
      40.0       5.4
      41.0      50.4
      42.0       5.8
      43.0       8.7
      49.0       1.5
      50.0       1.3
      51.0       4.6
      52.0       3.1
      53.0      17.7
      54.0       5.7
      55.0      21.0
      56.0       1.8
      63.0       3.9
      65.0       8.3
      66.0       5.4
      67.0     100.0
      68.0      53.1
      69.0      23.6
      70.0       1.4
      75.0       1.3
      77.0       7.4
      78.0       1.7
      79.0      18.5
      80.0       3.5
      81.0      39.0
      82.0      19.9
      83.0       2.4
      91.0       6.3
      92.0       1.0
      93.0       7.4
      94.0       2.1
      95.0      34.3
      96.0       5.7
     102.0       1.1
     105.0       2.3
     107.0      11.0
     108.0       1.7
     109.0      27.3
     110.0       6.1
     116.0       1.0
     121.0       2.1
     123.0       8.3
     124.0       1.0
     129.0       8.2
     130.0       6.7
     131.0       3.3
     132.0       2.2
     136.0       1.4
     143.0       9.5
     144.0       1.3
     145.0       3.2
     157.0       1.1
     171.0       1.5

400 MHz in CDCl3

¹H NMR	399.65 MHz
C₁₀ H₁₇ Cl	0.05 ml : 0.5 ml CDCl₃
10-chloro-3-decyne

    Assign.     Shift(ppm)

      A             3.534
      B             2.16
      C             2.15
      D             1.779
      E             1.49
      F             1.43
      G             1.111

     Hz     ppm     Int.

   1419.43   3.552    419
   1412.72   3.535    786
   1406.01   3.519    441
    864.75   2.164    423
    862.79   2.159    267
    860.60   2.154    232
    857.91   2.147    481
    857.18   2.145    419
    851.68   2.132    228
    712.52   1.783    214
    573.97   1.437    290
    572.75   1.434    284
    570.19   1.427    361
    567.38   1.420    327
    451.66   1.131    461
    444.09   1.112   1000
    436.65   1.093    436

in CDCl3