1852-16-0

N-(N-丁氧基甲基)丙烯酰胺(1852-16-0)質(zhì)譜(MS)

產(chǎn)品名稱:N-(N-丁氧基甲基)丙烯酰胺

CAS:1852-16-0

分子式:C8H15NO2

分子量: 157.21

InChI:InChI=1S/C8H15NO2/c1-3-5-6-11-7-9-8(10)4-2/h4H,2-3,5-7H2,1H3,(H,9,10)

InChIKey: UTSYWKJYFPPRAP-UHFFFAOYSA-N

Smiles:C(NCOCCCC)(=O)C=C

Mass

MS-NW-1084          
N-(butoxymethyl)acrylamide
C8H15NO2            (Mass of molecular ion:    157)

   Source Temperature: 250 °C
   Sample Temperature: 170 °C
   Reservoir, 75 eV

      15.0       1.6
      18.0       1.6
      19.0       1.1
      25.0       1.2
      26.0       8.5
      27.0      60.9
      28.0      15.1
      29.0      13.3
      30.0       4.0
      31.0      34.9
      32.0       2.6
      33.0       3.2
      37.0       1.1
      38.0       1.5
      39.0       7.3
      40.0       2.1
      41.0      33.3
      42.0      14.1
      43.0      24.4
      44.0       2.1
      45.0       3.1
      46.0       1.7
      53.0       1.5
      54.0       1.7
      55.0     100.0
      56.0      40.7
      57.0      10.1
      58.0       1.3
      71.0       1.1
      72.0       1.1
      73.0       1.2
      83.0       5.5
      84.0      41.5
      85.0      13.0
      87.0       1.3
     100.0      15.7
     101.0       1.1

90 MHz in CDCl3

¹H NMR	89.56 MHz
C₈ H₁₅ N O₂	0.04 ml : 0.5 ml CDCl₃
N-(butoxymethyl)acrylamide

    Assign.     Shift(ppm)

      A             7.0
      B             6.309
      C             6.218
      D             5.706
      E             4.801
      F             3.501
      G             1.53
      J             1.36
      K             0.92

     Hz     ppm     Int.

    578.63   6.461    116
    565.06   6.310    646
    563.13   6.288    567
    561.81   6.274    688
    554.44   6.191    617
    537.63   6.004    144
    515.94   5.761    438
    512.69   5.725    360
    507.31   5.665    258
    504.06   5.629    254
    433.38   4.839   1000
    426.63   4.764    963
    320.38   3.578    258
    318.88   3.561    153
    314.00   3.507    776
    307.63   3.435    358
    144.69   1.616    114
    135.44   1.513    222
    132.94   1.485    312
    119.25   1.332    169
     87.38   0.976    435
     80.88   0.904    986
     73.44   0.821    151

in CDCl3