19764-96-6

碘化-1,1ˊ,3,3,3ˊ,3ˊ-六甲基吲哚三羰花青(19764-96-6)核磁圖(¹HNMR)

產(chǎn)品名稱:碘化-1,1ˊ,3,3,3ˊ,3ˊ-六甲基吲哚三羰花青

CAS:19764-96-6

分子式:C29H33IN2

分子量: 536.49

¹HNMR

IR1

IR2

Mass

MS-NW-7761          
1,1',3,3,3',3'-hexamethylindotricarbocyanine iodide
C29H33IN2           (Mass of molecular ion:    536)

   Source Temperature: 220 °C
   Sample Temperature: 200 °C
   Direct, 75 eV

      15.0       3.4
      27.0       2.9
      28.0       1.2
      39.0       6.3
      41.0       2.4
      42.0       2.2
      50.0       3.2
      51.0       6.9
      52.0       2.2
      53.0       1.2
      62.0       2.4
      63.0       5.6
      64.0       1.9
      65.0       3.2
      74.0       2.7
      75.0       3.4
      76.0       4.0
      77.0       8.8
      78.0       2.4
      78.5       1.0
      79.0       1.8
      86.0       1.1
      87.0       1.4
      88.0       1.9
      89.0       5.5
      90.0       2.0
      91.0       4.6
     101.0       2.5
     102.0       5.5
     102.5       1.8
     103.0       3.6
     113.0       1.1
     114.0       1.0
     115.0      10.9
     116.0       4.9
     117.0       3.4
     118.0       1.7
     126.0       1.1
     127.0       9.5
     128.0       7.0
     129.0       3.4
     130.0       4.9
     131.0       2.3
     132.0       1.2
     139.0       1.4
     140.0       2.0
     141.0       2.3
     142.0      16.8
     143.0      12.4
     144.0       5.2
     145.0       1.6
     150.0       1.0
     151.0       2.8
     152.0       4.0
     153.0       1.6
     154.0       1.9
     156.0       5.5
     157.0       8.5
     158.0     100.0
     159.0      16.3
     160.0       3.9
     163.0       1.2
     164.0       1.4
     165.0       2.7
     166.0       1.2
     167.0       1.1
     170.0       1.2
     171.0       1.4
     172.0      13.3
     173.0      45.6
     174.0       6.2
     175.0       1.1
     176.0       2.3
     177.0       2.4
     178.0       8.1
     179.0       6.0
     180.0       9.7
     181.0       1.8
     186.0       1.3
     187.0       4.7
     189.0       1.1
     190.0       2.9
     191.0       3.3
     192.0       2.0
     193.0       1.5
     194.0       1.1
     202.0       1.1
     203.0       1.7
     204.0       7.5
     205.0       3.8
     206.0      59.6
     207.0      10.9
     208.0       1.4
     218.0       1.5
     220.0       8.0
     221.0      25.2
     222.0       6.8
     223.0       1.0
     234.0       1.6
     235.0       2.2
     236.0       1.3
     237.0       1.7
     248.0       1.6
     249.0       1.2
     262.0       1.2
     393.0       2.1
     394.0       1.4
     408.0       5.3
     409.0       1.7
     410.0       1.3

400 MHz in CDCl3

¹H NMR	399.65 MHz
C₂₉ H₃₃ I N₂	0.028 g : 0.5 ml CDCl₃
1,1',3,3,3',3'-hexamethylindotricarbocyanine iodide

    Assign.     Shift(ppm)

      A             7.85
      B             7.73
      C             7.36
      D             7.34
      E             7.204
      F             7.129
      G             6.63
      J             6.24
      K             3.660
      L             1.691

     Hz     ppm     Int.

   3138.67   7.854     22
   2952.39   7.388     66
   2951.29   7.385     74
   2944.46   7.368    134
   2943.60   7.366    153
   2937.01   7.349    206
   2935.91   7.347    220
   2929.44   7.331    173
   2885.50   7.221    103
   2878.54   7.203    153
   2878.05   7.202    154
   2871.09   7.185     65
   2870.61   7.183     65
   2853.03   7.139    118
   2845.09   7.119    102
   2651.37   6.635     29
   2499.02   6.254     30
   2486.08   6.221     29
   1463.01   3.661    427
    675.78   1.691   1000

KBr disc